Determination of the Region of Thermal Stability of the Size and Phase Composition of Silver-Sulfide Semiconductor Nanoparticles
- Authors: Sadovnikov S.I.1, Vovkotrub E.G.2
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Affiliations:
- Institute of Solid-State Chemistry, Ural Branch, Russian Academy of Sciences
- Institute of High-Temperature Electrochemistry, Ural Branch, Russian Academy of Sciences
- Issue: Vol 52, No 13 (2018)
- Pages: 1763-1769
- Section: Fabrication, Treatment, and Testing of Materials and Structures
- URL: https://journals.rcsi.science/1063-7826/article/view/204946
- DOI: https://doi.org/10.1134/S1063782618130146
- ID: 204946
Cite item
Abstract
The region of thermal stability of the size and phase composition of silver sulfide (Ag2S) nanoparticles is determined. Nanopowders consisting of Ag2S nanoparticles 475–50 nm in sizes are produced by chemical deposition from aqueous solutions. To analyze the thermal stability of Ag2S nanoparticles, nanocrystalline powders are annealed upon heating from room temperature to 453 K. Annealing at temperatures of up to 453 K does not induce the growth of nanoparticles, nor any change in their phase composition, which allows the conclusion that this temperature range is the range of thermal stability of the nanostate of silver sulfide.
About the authors
S. I. Sadovnikov
Institute of Solid-State Chemistry, Ural Branch, Russian Academy of Sciences
Author for correspondence.
Email: sadovnikov@ihim.uran.ru
Russian Federation, Yekaterinburg, 620990
E. G. Vovkotrub
Institute of High-Temperature Electrochemistry, Ural Branch, Russian Academy of Sciences
Email: sadovnikov@ihim.uran.ru
Russian Federation, Yekaterinburg, 620137