Catalytic Cycloaminomethylation of Aminobenzamides with 1,3-Bis[dimethylamino(methoxy)methyl]thiourea

R. R. Khairullina; T. V. Tyumkina; A. R. Geniyatova; M. F. Abdullin; A. G. Ibragimov

doi:10.1134/S1070363219030022

Catalytic Cycloaminomethylation of Aminobenzamides with 1,3-Bis[dimethylamino(methoxy)methyl]thiourea

作者: Khairullina R.¹, Tyumkina T.¹, Geniyatova A.¹, Abdullin M.², Ibragimov A.¹
隶属关系:
1. Institute of Petrochemistry and Catalysis of the Russian Academy of Sciences
2. Ufa Institute of Chemistry of the Russian Academy of Sciences
期: 卷 89, 编号 3 (2019)
页面: 378-384
栏目: Article
URL: https://journals.rcsi.science/1070-3632/article/view/222776
DOI: https://doi.org/10.1134/S1070363219030022
ID: 222776

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Efficient methods of the synthesis of cyclophanes containing the thiourea moiety via the reaction of o-, m-, and p-aminobenzamides with 1,3-bis(dimethylaminomethyl)thiourea or 1,3-bis(methoxymethyl)thiourea using NiCl₂·6H₂O and SmCl₃·6H₂O as catalysts have been developed.