Catalytic Cycloaminomethylation of Aminobenzamides with 1,3-Bis[dimethylamino(methoxy)methyl]thiourea
- Authors: Khairullina R.R.1, Tyumkina T.V.1, Geniyatova A.R.1, Abdullin M.F.2, Ibragimov A.G.1
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Affiliations:
- Institute of Petrochemistry and Catalysis of the Russian Academy of Sciences
- Ufa Institute of Chemistry of the Russian Academy of Sciences
- Issue: Vol 89, No 3 (2019)
- Pages: 378-384
- Section: Article
- URL: https://journals.rcsi.science/1070-3632/article/view/222776
- DOI: https://doi.org/10.1134/S1070363219030022
- ID: 222776
Cite item
Abstract
Efficient methods of the synthesis of cyclophanes containing the thiourea moiety via the reaction of o-, m-, and p-aminobenzamides with 1,3-bis(dimethylaminomethyl)thiourea or 1,3-bis(methoxymethyl)thiourea using NiCl2·6H2O and SmCl3·6H2O as catalysts have been developed.
About the authors
R. R. Khairullina
Institute of Petrochemistry and Catalysis of the Russian Academy of Sciences
Author for correspondence.
Email: ink@anrb.ru
Russian Federation, pr. Oktyabrya 141, Ufa, 450075
T. V. Tyumkina
Institute of Petrochemistry and Catalysis of the Russian Academy of Sciences
Email: ink@anrb.ru
Russian Federation, pr. Oktyabrya 141, Ufa, 450075
A. R. Geniyatova
Institute of Petrochemistry and Catalysis of the Russian Academy of Sciences
Email: ink@anrb.ru
Russian Federation, pr. Oktyabrya 141, Ufa, 450075
M. F. Abdullin
Ufa Institute of Chemistry of the Russian Academy of Sciences
Email: ink@anrb.ru
Russian Federation, pr. Oktyabrya 71, Ufa, 450054
A. G. Ibragimov
Institute of Petrochemistry and Catalysis of the Russian Academy of Sciences
Email: ink@anrb.ru
Russian Federation, pr. Oktyabrya 141, Ufa, 450075