Simultaneous determination of aliphatic acids and aldehydes in aqueous media by reaction gas chromatography
- Авторы: Pervova M.1, Chizhov D.1, Saloutin V.1
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Учреждения:
- Institute of Organic Synthesis, Ural Branch
- Выпуск: Том 71, № 10 (2016)
- Страницы: 1041-1045
- Раздел: Articles
- URL: https://journals.rcsi.science/1061-9348/article/view/182113
- DOI: https://doi.org/10.1134/S1061934816100099
- ID: 182113
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Аннотация
A procedure is developed for the gas chromatographic determination of lower aldehydes as dibutoxyalkanes and carboxylic acids as butyl esters by the reaction with tributyl borate in an aqueous medium. Derivatization conditions were optimized. The procedure was used to determine side products in glyoxal synthesized by the catalytic oxidation of ethylene glycol.
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Об авторах
M. Pervova
Institute of Organic Synthesis, Ural Branch
Автор, ответственный за переписку.
Email: pervova@ios.uran.ru
Россия, ul. S. Kovalevskoi 22/Akademicheskaya 20, Yekaterinburg, 620990
D. Chizhov
Institute of Organic Synthesis, Ural Branch
Email: pervova@ios.uran.ru
Россия, ul. S. Kovalevskoi 22/Akademicheskaya 20, Yekaterinburg, 620990
V. Saloutin
Institute of Organic Synthesis, Ural Branch
Email: pervova@ios.uran.ru
Россия, ul. S. Kovalevskoi 22/Akademicheskaya 20, Yekaterinburg, 620990
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