Email this article Simultaneous determination of aliphatic acids and aldehydes in aqueous media by reaction gas chromatography
- Authors: Pervova M.G.1, Chizhov D.L.1, Saloutin V.I.1
-
Affiliations:
- Institute of Organic Synthesis, Ural Branch
- Issue: Vol 71, No 10 (2016)
- Pages: 1041-1045
- Section: Articles
- URL: https://journals.rcsi.science/1061-9348/article/view/182113
- DOI: https://doi.org/10.1134/S1061934816100099
- ID: 182113
Cite item
Open Access
Access granted
Subscription Access
Abstract
A procedure is developed for the gas chromatographic determination of lower aldehydes as dibutoxyalkanes and carboxylic acids as butyl esters by the reaction with tributyl borate in an aqueous medium. Derivatization conditions were optimized. The procedure was used to determine side products in glyoxal synthesized by the catalytic oxidation of ethylene glycol.
About the authors
M. G. Pervova
Institute of Organic Synthesis, Ural Branch
Author for correspondence.
Email: pervova@ios.uran.ru
Russian Federation, ul. S. Kovalevskoi 22/Akademicheskaya 20, Yekaterinburg, 620990
D. L. Chizhov
Institute of Organic Synthesis, Ural Branch
Email: pervova@ios.uran.ru
Russian Federation, ul. S. Kovalevskoi 22/Akademicheskaya 20, Yekaterinburg, 620990
V. I. Saloutin
Institute of Organic Synthesis, Ural Branch
Email: pervova@ios.uran.ru
Russian Federation, ul. S. Kovalevskoi 22/Akademicheskaya 20, Yekaterinburg, 620990
