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Vol 60, No 3 (2017)

General Problems of Metrology and Measurement Technique

Use of Mixtures of Distributions for Stochastic Prediction of the Behavior of the Parameters of Engineering Objects

Sysoev Y.S.

Abstract

An algorithm is proposed for using mixtures of distributions with the same names and with different names for stochastic prediction of changes in the numerical parameters of engineering objects during operation. The class of practical problems for possible prediction using mass servicing systems is expanded.

Measurement Techniques. 2017;60(3):203-210
pages 203-210 views

Article

Multichannel Measurement System for Data Acquisition From Silicon Photomultiplier Arrays

Yanin A.F., Dzaparova I.M., Volchenko V.I., Gorbacheva E.A., Kurenya A.N., Petkov V.B.

Abstract

The MMIS-32 scaled multichannel measurement system, which is based on 32-channel charge-to-digital converters and has been developed and built, is described here. This system is intended for data acquisition from arrays of silicon photomultipliers used as multichannel photosensors in scintillation detectors. The basic parameters of the measurement system are presented.

Measurement Techniques. 2017;60(3):211-215
pages 211-215 views

Measurement of the Height of Nanorelief Elements by the Method of Three-Dimensional Reconstruction in a Scanning Electron Microscope

Darznek S.A., Karabanov D.A., Kuzin A.Y., Mityukhlyaev V.B., Todua P.A., Filippov M.N.

Abstract

Comparative measurements of the height of the nanorelief steps of the surface of a silicon wafer by methods of three-dimensional reconstruction using a scanning electron microscope and profilometry were carried out. To realize the method of three-dimensional reconstruction, an islet gold film is formed on the surface of the test sample. The AlphaStep D-600 profiler is calibrated with a KTS-4500 QS step height gauge. The coincidence of the results of measurements with the methods of three-dimensional reconstruction and profilometry is established. The possibilities of reducing the uncertainty of the measurement results by the method of three-dimensional reconstruction were analyzed.

Measurement Techniques. 2017;60(3):220-225
pages 220-225 views

Use of Information Redundancy in Optical Digital Measurement Systems with 2D Sensor

Korolev A.N., Lukin A.Y., Polishchuk G.S.

Abstract

A unified approach to the management of measurements in optical digital measurement systems with 2D sensor is considered. The proposed approach is based on exhaustive use of information redundancy, that is, the use of coordinate information about the object distributed over the entire field of the image. The efficiency of the approach is demonstrated for the case of autocollimators. Results of simulation and experiment that confirm that the precision of devices may be increased through the use of a multi-element mark and coordinate information over the entire information field are presented. The basic problems that arise in the development and introduction of the approach are formulated.

Measurement Techniques. 2017;60(3):242-247
pages 242-247 views

Estimating the Error Component Associated with the Selection of a Gas Flow Model in Critical Nozzles

Chesnokov V.I., Ipolitov B.A.

Abstract

A more accurate model has been developed for an ideal compressed gas flow in a critical nozzle used as a standard for volumetric flow rate. An error assessment is carried out for the inadequacy of the classical model of a critical nozzle that is applied to obtaining the actual value of the volumetric flow rate produced by a nozzle in operating conditions. It is shown that the error of model inadequacy must be considered to be in the upper bounds region of the effective measurement ranges of gas counters when calibrating them by means of volumetric flow rate standards on critical nozzles.

Measurement Techniques. 2017;60(3):254-261
pages 254-261 views

A New Technique for Measuring the Nonlinear Distortion of Analog Multipliers

Zen’kovich A.V., Ballo V.L., Dobrovol’skii V.B.

Abstract

The advantages of a new technique for measuring the nonlinear distortions of analog multipliers of signals by sensitivity, resolving power, frequency range and the implementation rate are experimentally confirmed.

Measurement Techniques. 2017;60(3):279-282
pages 279-282 views

Upgraded Microwave Radio Thermometer Input Unit for Remote Temperature Measurement of a Biological Object

Filatov A.V., Anishin M.N., Gazitov S.R., Tarasov S.E., Utkin B.V., Shibel’gut A.A.

Abstract

A modernized input unit of a microwave radio thermometer designed for the study of biological media is described. In this unit, a coupler is applied on the connected transmission lines. A part of the high-frequency signal of the noise generator branches from the main channel into the working arms of the secondary channel with different coefficients of transient attenuation, whose difference determines the range of measurements. Modeling the coupler parameters enables the creation of radio thermometers with specified measurement ranges.

Measurement Techniques. 2017;60(3):283-290
pages 283-290 views

Sensitivity of Broad-Band Piezosorption Moisture Sensors for Nondestructive Monitoring of Organic Solvents

Voronova T.S., Lipnin Y.A., Mazur V.G., Pudalov A.D.

Abstract

A model of the static characteristic of a broad-band piezosorption moisture sensor for nondestructive monitoring of organic solvents is proposed. Based on the criterion of maximum sensitivity of the sensors, optimum ratios are proposed for the mass fractions of sorbents deposited on a quartz plate for measuring the relative moisture content of organic solvents for relative concentrations of 0–1 rel. units. Experimental studies are used to determine the model parameters for different ratios of the mass fractions of sorbents.

Measurement Techniques. 2017;60(3):300-304
pages 300-304 views

Method for Calibrating Commercial Microwave Hygrometers

Kovaleva A.A., Saitov R.I., Zaporozhets A.S., Parfenova E.G.

Abstract

A method is proposed for calibrating microwave hygrometers with lower error in determining the difference between the true conversion function and the nominal calibration dependence attributed to a series of hygrometers. The proposed method can be used to extend the results of calibrating a single hygrometer with a natural sample of material to an entire series of hygrometers.

Measurement Techniques. 2017;60(3):305-308
pages 305-308 views

Nanometrology

Pulsed Laser Ablation for Obtaining Contrast Agents Based on Dysprosium Oxide (Dy2O3) Nanoparticles

Barshutina M.N., Barchanski A.

Abstract

The use of the pulsed laser ablation method is proposed for obtaining solutions based on Dy2O3-nanoparticles for T2 MRI contrast agents at high magnetic fields. It has been demonstrated that the PLA method can help simplify and shorten the duration of obtaining stable Dy2O3 nanoparticle-based colloids, the relaxivity of which exceeds the relaxivity values of commercially-available MRI contrast agents.

Measurement Techniques. 2017;60(3):216-219
pages 216-219 views

Linear and Angular Measurements

Measurement of Angles of Polyhedral Prisms on the State Primary Standard Get 22-2014 for a Flat Angle Unit

Chekirda K.V., Shur V.L., Kos’mina M.A., Leibengardt G.I., Lukin A.Y.

Abstract

An installation for measuring the angles of polyhedral prisms is considered, in which autocollimators with digital registration of the coordinates of the optical mark are applied. Algorithms for solving systems of equations for the determination of angles by the method of aggregate measurements with the help of two and three autocollimators are described. The errors in the measurements are calculated and compared with the results of experimental measurements of the angles of polyhedral prisms.

Measurement Techniques. 2017;60(3):226-234
pages 226-234 views

Optophysical Measurements

Metrology of Single Photons for Quantum Information Technologies

Magnitskii S.A., Frolovtsev D.N., Agapov D.P., Demin A.V., Krutikov V.N., Levin G.G.

Abstract

A new approach is proposed for the metrology of optical measurements – the quantum metrology of photons. The specific nature of measurements of quantum polarization states of single and polarization-entangled photons is examined. The fundamental objectives of the modern metrology of photons are formulated.

Measurement Techniques. 2017;60(3):235-241
pages 235-241 views

Mechanical Measurements

Method for Measuring Cutting Force During Ultrahigh-Speed Metal Processing

Korneeva V.M., Korneev S.S.

Abstract

A method has been developed to measure the cutting force during ultrahigh-speed metal processing, making it possible to estimate this force during processing. A specialized measuring transducer was designed and a methodology was created to interpret the transducer signal directly as it is being recorded by registration equipment.

Measurement Techniques. 2017;60(3):248-253
pages 248-253 views

Ionizing Radiation Measurements

Primary Transducer for Measuring Flux Density of Charged Particles

Trofimchuk S.G., Tsvetkov I.I., Oborin A.V., Villevalde A.Y.

Abstract

The design and main metrological characteristics are presented for a Faraday cup type primary transducer for measuring electron flux density with maximum energy to 20 MeV and protons with maximum energy to 100 MeV, in the range 1·105–1·1010 cm–2·sec–1, by transfer the units to measuring instruments incorporated into heliogeophysical equipment systems.

Measurement Techniques. 2017;60(3):262-266
pages 262-266 views

Electromagnetic Measurements

Algorithm for Monitoring the State of Insulation in Voltage Measurement Transformers in the Generator Voltage Circuit of Power Plants

Gevorkyan V.M., Krayushkin K.V.

Abstract

An algorithm for monitoring the state of insulation in voltage measurement transformers in the voltage generation circuit of power plants is discussed. A principle for constructing a monitoring device of this kind is proposed and its reliability for monitoring the state of the voltage measurement transformer is evaluated.

Measurement Techniques. 2017;60(3):267-273
pages 267-273 views

Radio Measurements

Features of the Determination of the Complex Transfer Coefficients of a Frequency Converter by Methods of Combined Measurements

Frolov D.R., Babenko A.A., Biryuk A.E., Kozhevnikov V.V., Svidlov A.A.

Abstract

We consider causes that limit the accuracy of the measurements of complex transfer coefficients (CTCs) of a frequency converter by methods based on various combinations of parallel and series connections of the indicated converters. It is impossible to carry out such measurements without using a reciprocal frequency converter. It was established that the limiting accuracy of the given measurement methods was determined by the degree of reciprocity of at least one of the frequency converters.

Measurement Techniques. 2017;60(3):274-278
pages 274-278 views

Medical and Biological Measurements

Analysis of Methods and Means of Measuring Catalytic Activity of Biologically and Chemically Active Substances

Kudeyarov Y.A., Kulyabina E.V., Melkova O.N., Zelenkova M.V., Pan’kov A.N., Pakharukov I.Y.

Abstract

Methods and instrumentation for measuring catalytic activity that may be useful in the development of standards are analyzed. Analysis showed that, with all the variety of methods and instruments for measuring catalytic activity, during the development of the standard it is necessary to fulfill a set of mandatory requirements in the selection of objects for the study (catalysts), methods, and measuring instruments.

Measurement Techniques. 2017;60(3):291-296
pages 291-296 views

Physicochemical Measurements

Metrological Problems of Moisture Metering Of Building Materials

Roife V.S., Verkhovskii A.A., Zaporozhets A.S., Parfenova E.G., Kozynchenko V.B.

Abstract

Certain aspects of metrological assurance of building materials moisture metering are presented. Verification of dielcometric hydrometers using reference materials is considered. The advantages and drawbacks of sample simulators and reference materials based on natural substances are demonstrated. A broad range of standard samples and sample simulators is created in order to improve the system of metrological assurance of the building materials branch and regulatory documents that define the methods and means of verification of the moisture meters used with building materials are developed.

Measurement Techniques. 2017;60(3):297-299
pages 297-299 views