Synthesis and thermal analysis of a Ni(II) complex of nicotinamide

G. A. Gamov; M. N. Zavalishin; S. V. Dushina; V. A. Sharnin

doi:10.1134/S1070363217030380

Synthesis and thermal analysis of a Ni(II) complex of nicotinamide

Autores: Gamov G.¹, Zavalishin M.¹, Dushina S.¹, Sharnin V.¹
Afiliações:
1. Ivanovo State University of Chemistry and Technology (ISUCT)
Edição: Volume 87, Nº 3 (2017)
Páginas: 613-618
Seção: Selected articles originally published in Russian in Rossiiskii Khimicheskii Zhurnal (Russian Chemistry Journal)
URL: https://journals.rcsi.science/1070-3632/article/view/219060
DOI: https://doi.org/10.1134/S1070363217030380
ID: 219060

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Nickel(II) bisnicotinamide sulfate was synthesized, isolated, and studied by means of FTIR spectroscopy, thermogravimetry, and differential scanning calorimetry with simultaneous mass-spectrometry analysis of pyrolysis products. The order the molecules are evolved from the coordination compound during thermal treatment is determined. The total heat effects of the processes involved in pyrolysis are estimated.