Synthesis and thermal analysis of a Ni(II) complex of nicotinamide

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Abstract

Nickel(II) bisnicotinamide sulfate was synthesized, isolated, and studied by means of FTIR spectroscopy, thermogravimetry, and differential scanning calorimetry with simultaneous mass-spectrometry analysis of pyrolysis products. The order the molecules are evolved from the coordination compound during thermal treatment is determined. The total heat effects of the processes involved in pyrolysis are estimated.

About the authors

G. A. Gamov

Ivanovo State University of Chemistry and Technology (ISUCT)

Author for correspondence.
Email: injures@yandex.ru
Russian Federation, pr. Sheremetevskii 7, Ivanovo, 153000

M. N. Zavalishin

Ivanovo State University of Chemistry and Technology (ISUCT)

Email: injures@yandex.ru
Russian Federation, pr. Sheremetevskii 7, Ivanovo, 153000

S. V. Dushina

Ivanovo State University of Chemistry and Technology (ISUCT)

Email: injures@yandex.ru
Russian Federation, pr. Sheremetevskii 7, Ivanovo, 153000

V. A. Sharnin

Ivanovo State University of Chemistry and Technology (ISUCT)

Email: injures@yandex.ru
Russian Federation, pr. Sheremetevskii 7, Ivanovo, 153000


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