Synthesis and thermal analysis of a Ni(II) complex of nicotinamide
- Authors: Gamov G.A.1, Zavalishin M.N.1, Dushina S.V.1, Sharnin V.A.1
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Affiliations:
- Ivanovo State University of Chemistry and Technology (ISUCT)
- Issue: Vol 87, No 3 (2017)
- Pages: 613-618
- Section: Selected articles originally published in Russian in Rossiiskii Khimicheskii Zhurnal (Russian Chemistry Journal)
- URL: https://journals.rcsi.science/1070-3632/article/view/219060
- DOI: https://doi.org/10.1134/S1070363217030380
- ID: 219060
Cite item
Abstract
Nickel(II) bisnicotinamide sulfate was synthesized, isolated, and studied by means of FTIR spectroscopy, thermogravimetry, and differential scanning calorimetry with simultaneous mass-spectrometry analysis of pyrolysis products. The order the molecules are evolved from the coordination compound during thermal treatment is determined. The total heat effects of the processes involved in pyrolysis are estimated.
About the authors
G. A. Gamov
Ivanovo State University of Chemistry and Technology (ISUCT)
Author for correspondence.
Email: injures@yandex.ru
Russian Federation, pr. Sheremetevskii 7, Ivanovo, 153000
M. N. Zavalishin
Ivanovo State University of Chemistry and Technology (ISUCT)
Email: injures@yandex.ru
Russian Federation, pr. Sheremetevskii 7, Ivanovo, 153000
S. V. Dushina
Ivanovo State University of Chemistry and Technology (ISUCT)
Email: injures@yandex.ru
Russian Federation, pr. Sheremetevskii 7, Ivanovo, 153000
V. A. Sharnin
Ivanovo State University of Chemistry and Technology (ISUCT)
Email: injures@yandex.ru
Russian Federation, pr. Sheremetevskii 7, Ivanovo, 153000