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Vol 83, No 2 (2019)

Article

Multilayer X-Ray Image-Forming Optics

Chkhalo N.I., Salashchenko N.N.

Abstract

An overview is presented of the current state of research underway at the Institute for the Physics of Microstructures in the field of multilayered X-ray imaging optics. New ways of studying the surfaces of mirror substrates and aberrations of optical systems are described, along with the ion-beam technology of super-polishing, aspherization, and correcting local errors in shape. The development of new diagnostic methods is described, as are the obtained record reflection coefficients of multilayer interference mirrors based on beryllium.

Bulletin of the Russian Academy of Sciences: Physics. 2019;83(2):105-111
pages 105-111 views

The SRXFA Station on the VEPP-4M Storage Ring

Legkodymov A.A., Kuper K.E., Kolmogorov Y.P., Baranov G.N.

Abstract

A description is given of the SRXFA synchrotron radiation station on the VEPP-4M storage ring at the Siberian Synchrotron and Terahertz Radiation Center. The station is intended to develop and implement SRXFA technology in the hard X-ray photon (40–120 keV) range. The main parameters of the station are given, along with its layout, its monochromatic system, and its detector. The X-ray fluorescence spectrum obtained at the SRXFA station on the VEPP-4M storage ring at an excitation energy of 112 keV is presented. Results obtained at the station on the minimum detection limits for rare-earth elements are presented.

Bulletin of the Russian Academy of Sciences: Physics. 2019;83(2):112-115
pages 112-115 views

Feedback Suppression of the Fast Vertical Oscillations of VEPP-3 SR Beam

Fedotov M.G., Mishnev S.I., Ljangasov I.D.

Abstract

Experiments are performed on suppressing vertical oscillations of the synchrotron radiation beam of the VEPP-3 storage ring by introducing fast feedback. The detector, based on pin photodiodes with an electronic signal processing path and an electromechanical system of automatic alignment, is a beam position sensor. A pair of iron-free coils is used as a quick corrector. 30 dB suppression of oscillations with a frequency of 50 Hz and 25 dB suppression of powerful interference with a frequency of 690 Hz are obtained in experiments.

Bulletin of the Russian Academy of Sciences: Physics. 2019;83(2):116-120
pages 116-120 views

Radiation-Generating Devices for Domestic Sources of Synchrotron Radiation with Extremely Low Emittance

Zorin A.V., Mezentsev N.A., Zolotarev K.V., Shkaruba V.A.

Abstract

It is planned to construct a network of national sources of synchrotron radiation with extremely low emittance in Russia in the near future, known as the SSRS-4 (Fourth Generation Specialized Source of Synchrotron Radiation program). In this work, modern and promising methods for using synchrotron radiation are described from the viewpoint of insertion devices for generating synchrotron radiation.

Bulletin of the Russian Academy of Sciences: Physics. 2019;83(2):121-123
pages 121-123 views

Forming and Testing High-Aspect Anti-Scattering Grids for Flash X-Ray Radiography

Goldenberg B.G., Nazmov V.P., Palchikov E.I., Lemzyakov A.G., Dolgikh A.V., Mishnev S.I.

Abstract

The applicability of high-aspect anti-scattering grids for correcting the radiation pattern of pulsed X-ray tubes in the photon energy range of 20–200 keV is considered. Techniques for fabricating and testing metal anti-scattering rasters are described. Experimental studies of changes in X-ray radiation patterns using anti-scatter rasters are cited.

Bulletin of the Russian Academy of Sciences: Physics. 2019;83(2):124-128
pages 124-128 views

Designing a Technological Station for Synchrotron Radiation on the VEPP-4M

Goldenberg B.G., Rakshun Y.V., Bugaev S.V., Meshkov O.I., Tsybulya S.V.

Abstract

A technological station for synchrotron radiation (referred to below as the TSSR) is created on Channel 1 of synchrotron radiation (SR) output on the VEPP-4M storage ring. The new station is designed for practical study of the basics of synchrotron research conducted by university students. The modular construction of the station allows us to change its equipment, test different research techniques and new equipment, and perform some auxiliary experiments. The design of the station, the radiation characteristics relative to other active SR stations, and the main training programs are described.

Bulletin of the Russian Academy of Sciences: Physics. 2019;83(2):129-133
pages 129-133 views

Results from X-Ray Microtomography Studies of Gallbladder Stones

Asadchikov V.E., Buzmakov A.V., Dyachkova I.G., Zolotov D.A., Ivanova A.G., Krivonosov Y.S., Pantyushov V.V., Saifutdinov R.G., Voloshin A.E.

Abstract

Results are presented from in vitro investigations of gallbladder stones using X-ray microtomography with radiation energy of 17.5 keV. Linear absorption coefficients of gallstones that were obtained in the experiment are compared to corresponding coefficients calculated using reference data for pure cholesterol. The possibility of using X-ray microtomography to investigate the morphological structure of concrements is demonstrated. The stones are found to have cavities and layered formations. The phase composition of the stones is determined via powder diffraction.

Bulletin of the Russian Academy of Sciences: Physics. 2019;83(2):134-139
pages 134-139 views

Planar THz FELs Based on Intense Parallel Sheet Electron Beams and Intracavity Wave Scattering

Arzhannikov A.V., Ginzburg N.S., Zaslavsky V.Y., Kalinin P.V., Peskov N.Y., Sandalov E.S., Sergeev A.S., Sinitsky S.L., Stepanov V.D.

Abstract

A design for a planar FEL operating in the terahertz frequency range at the multimegawatt power level is being jointly developed at the ELMI accelerator by the Budker Institute of Nuclear Physics and the Institute of Applied Physics. The FEL oscillator is driven by parallel intense sheet electron beams of moderately relativistic energy, and transitions to the above frequency range via a two-stage cascade scheme. The first beam generates a powerful millimeter pump wave, which then travels through special waveguides to the parallel channel and is scattered by the second beam into a wave of terahertz radiation. Various possible arrangements of the FEL scheme are discussed, and results from their simulation are presented. The results from cold tests of the FEL’s electrodynamic system are reported.

Bulletin of the Russian Academy of Sciences: Physics. 2019;83(2):140-145
pages 140-145 views

Laboratory X-ray Microtomography: Ways of Processing Experimental Data

Buzmakov A.V., Asadchikov V.E., Zolotov D.A., Chukalina M.V., Ingacheva A.S., Krivonosov Y.S.

Abstract

Software is described for the preliminary processing of X-ray data that allow the spatial resolution of laboratory X-ray microtomographs to be improved.

Bulletin of the Russian Academy of Sciences: Physics. 2019;83(2):146-149
pages 146-149 views

A Hardware and Software System for Tomographic Research: Reconstruction via Regularization

Chukalina M.V., Ingacheva A.S., Buzmakov A.V., Krivonosov Y.S., Asadchikov V.E., Nikolaev D.P.

Abstract

Tomographic reconstruction by integral means preserves the prior information of a reconstructed image. It is difficult to reconstruct high-quality CT images by integral means if the measured parameters or object properties do not satisfy the requirements of the model used in reconstruction (few angles of rotation, angles that are not homogeneously distributed, the object containing regions critically different in absorption at the probing energy). Algebraic approaches are time-consuming. However, they allow consideration of the prior information of a setup or image. Results are prevented from a laboratory tomographic experiment on a test object. A highly absorbing inclusion is placed inside the object. A polychromatic beam is used. Results obtained using integral and algebraic reconstructions are compared. The reconstruction procedure is described in detail for the latter. The algebraic approach uses information on the presence of a highly absorbing region.

Bulletin of the Russian Academy of Sciences: Physics. 2019;83(2):150-154
pages 150-154 views

Developing an Undulator with a Variable Period for the First Stage of the Novosibirsk Free Electron Laser

Davidyuk I.V., Shevchenko O.A., Tcheskidov V.G., Vinokurov N.A., Getmanov Y.V.

Abstract

The development of a hybrid undulator with a small period-to-gap ratio (0.75) for the Novosibirsk Free Electron Laser (FEL) is described. The design of the undulator allows reconstruction of its period and a change in the number of poles. Since the configuration with permanent magnets can be scaled while preserving the field distribution, this design can be used both in installations operating in the terahertz range and for X-ray lasers. The results are presented from computer simulations and calculating the main parameters of the undulator.

Bulletin of the Russian Academy of Sciences: Physics. 2019;83(2):155-158
pages 155-158 views

A Computer-Based Test Bench for Modulating Terahertz FEL Radiation Power

Shevchenko O.A., Salikova T.V., Tararyshkin S.V., Getmanov Y.V., Veber S.L.

Abstract

A simple technique is proposed to modulate the output radiation power in a free-electron laser (FEL) oscillator that allows the average radiation power to be adjusted smoothly, and short (as brief as 35 μs) radiation macrobunches to be obtained. It is based on the periodic shift of the electron bunch phase with respect to that of an FEL radiation bunch stored in the optical cavity, resulting in lasing suppression. The phase shift frequency required to suppress lasing is relatively low and does not change the electron bunch repetition rate appreciably. A computer-based test bench is created to demonstrate the feasibility of the proposed technique. The test bench contains standard CAMAC blocks: a G0609 modulator timer and a G0601 clock generator. The electron bunch phase is shifted via programmable skipping of the reference frequency periods used to start the current modulator in the electron gun. The skipping is controlled by a computer program operating in the real-time mode. The clock generator is used to send synchronization signals to the radiation user’s equipment. The test bench is tested via EPR spectroscopy with a temporal resolution that allows the duration of the generated macrobunches to be estimated.

Bulletin of the Russian Academy of Sciences: Physics. 2019;83(2):159-162
pages 159-162 views

Compensating for Variation in Undulator Focusing when Tuning the Wavelength of the Novosibirsk FEL Radiation

Matveev A.S., Shevchenko O.A., Vinokurov N.A.

Abstract

Tuning the wavelength of the radiation on a free-electron laser (FEL) changes the strength of its undulators focusing. Two approaches to compensating for this effect are considered: conserving the transport matrix and matching the Twiss parameters. Both approaches are validated at the Novosibirsk FEL. As a result, beam propagation is maintained when retuning the wavelength of FEL radiation in the range of 120–130 μm.

Bulletin of the Russian Academy of Sciences: Physics. 2019;83(2):163-165
pages 163-165 views

Radiation Monitoring System of the Novosibirsk FEL

Salikova T.V., Vinokurov N.A., Petrichenkov M.V., Repkov A.V., Chudaev V.Y., Shevchenko O.A., Eksta V.V.

Abstract

The dosimetry system at the FEL facility registers the dose rates in workrooms and in the accelerator hall. The collected information is stored in the database, and the data is visualized in real time. The sensors installed in the accelerator hall are used for monitoring both radiation levels and beam losses on the walls of the vacuum chamber of the FEL’s transport tracks.

Bulletin of the Russian Academy of Sciences: Physics. 2019;83(2):166-168
pages 166-168 views

Spectroscopic Analysis of ZnS:Cu(Mn);Cl Nanofilms on Surfaces of Porous Alumina

Valeev R.G., Beltyukov A.N., Chukavin A.I., Vetoshkin V.M., Trigub A.L., Alalykin A.S., Kriventsov V.V.

Abstract

The electron and local atomic structures of ZnS:Cu(Mn);Cl nanofilms obtained via vacuum thermal deposition onto porous aluminum oxide are studied by means of X-ray photoelectron spectroscopy, XANES, and EXAFS. It is established that the pore diameter of a substrate has no effect on the local structure or phase composition of coatings.

Bulletin of the Russian Academy of Sciences: Physics. 2019;83(2):169-174
pages 169-174 views

Comparing and Assessing the Efficiency of Lasing for Different Configurations of the Electron Outcoupling System of the Novosibirsk Free Electron Laser

Getmanov Y.V., Gorbachev Y.I., Vinokurov N.A., Davidyuk I.V., Kubarev V.V., Shevchenko O.A.

Abstract

A scheme of electron radiation output is proposed to solve the problem of overheating of the optical resonator mirrors in free-electron lasers (FEL) with high average radiation power. Such a structure acts on the electron beam, which is initially grouped in the first section of the undulator due to interaction with the mode of the optical resonator. In subsequent sections, it rotates at a small angle relative to the optical axis while maintaining its grouping, and its coherent radiation goes beyond the limits of the resonator mode. The electron outcoupling system is installed on the last of the three lasers of the Novosibirsk FEL. It consists of three undulators, two quadrupoles, and dipole correctors located between them. There are thus two possible configurations, as the electron beam can be rotated in both the second and third undulator. Preliminary estimates of the radiation power are considered. Different configurations of the electron radiation output system of the Novosibirsk FEL are compared.

Bulletin of the Russian Academy of Sciences: Physics. 2019;83(2):175-179
pages 175-179 views

Conceptual Design for a Microfocus Beamline on the SKIF Synchrotron

Rashchenko S.V., Darin A.V., Rakshun Y.V.

Abstract

A design is proposed for a fourth-generation synchrotron beamline for investigating the structure and composition of a broad range of samples with high (submicron) spatial resolution.

Bulletin of the Russian Academy of Sciences: Physics. 2019;83(2):180-183
pages 180-183 views

Simulating Diffraction on a Series of Amplitude-Phase Masks for Experiments at the Novosibirsk Free Electron Laser

Kameshkov O.E., Knyazev B.A.

Abstract

The problem of calculating the electromagnetic field of directional radiation passing through a system of amplitude-phase masks arises in many studies. This work describes the WaveThruMasks software package written for planning and analyzing experiments on the terahertz radiation of the Novosibirsk free electron laser. An example is given of using the package to analyze the results from experimental studies of the diffraction of Bessel beams with orbital momentum on two-dimensional gratings.

Bulletin of the Russian Academy of Sciences: Physics. 2019;83(2):184-189
pages 184-189 views

Constructing Lithological/Geochemical Time Series in the Cross Sections of Bottom Sediments of Lake Karakel Using Data from Micro-XRF Scanning with a Beam of Synchrotron Radiation on the VEPP-3 Storage Ring

Darin A.V., Alexandrin M.Y., Grachev A.M., Solomina O.N., Darin F.A., Rakshun Y.V., Sorokoletov D.S.

Abstract

Cores of bottom sediments of Lake Karakel (Northern Caucasus) were obtained in 2010 and 2014 to perform geochemical studies for reconstructing the regional paleoclimate of the late Holocene. Solid samples of bottom sediments were scanned via micro-XRF with a step of 1 mm at the shared resource center of the Siberian Synchrotron and Terahertz Radiation Center. The contents of more than 20 elements were determined. The scan profiles are used to construct a single reference section with correction for a sediment layer dated via radiocarbon analysis, and to create a sediment core age–depth model.

Bulletin of the Russian Academy of Sciences: Physics. 2019;83(2):190-193
pages 190-193 views

Searching for Annually Stratified Bottom Sediments in Altai Mountain Lakes by Means of XRF Microanalysis Using Synchrotron Radiation

Darin A.V., Kalugin I.A., Babich V.V., Markovich T.I., Grachev A.M., Darin F.A., Rakshun Y.V., Sorokoletov D.S.

Abstract

Bottom sediments from Lake Kucherlinskoe that contain finely-laminated layers are studied using micro-XRF on synchrotron radiation beams from the VEPP-3 storage ring. Samples with visible layers are prepared as solid specimens impregnated with epoxy. The procedure for preparing the samples preserves the original structure and composition of the sediment. Scanning X-ray fluorescence microanalysis of the samples is performed on an experimental setup at the joint usage center of the Institute of Nuclear Physics, Siberian Synchrotron and Terahertz Radiation Center. Scan profiles with increments of 100 and 200 µm are obtained that contain data on the distribution of over 20 rock-forming and microelements. The experimental material is used to confirm the annual nature of the observed layering of sediments, estimate the rate of sedimentation, and construct a lithological and geochemical model of the sedimentation process.

Bulletin of the Russian Academy of Sciences: Physics. 2019;83(2):194-197
pages 194-197 views

Indicators of Oxic and Anoxic Conditions in the System of the Current Sedimentation of Saline Lake Shira (Khakassia), According to High-Resolution SR XRF Data on Bottom Sediments Frozen In Situ

Kalugin I.A., Darin A.V., Babich V.V., Markovich T.I., Rakshun Y.V., Darin F.A., Sorokoletov D.S., Rogozin D.Y.

Abstract

Frozen upper layers of the bottom sediment of Lake Shira are selected using special sampling equipment. Frozen samples and solid samples prepared from the upper layers of a sediment core are examined by means of X-ray fluorescence at the Local and Scanning X-Ray Fluorescence Elemental Analysis Station of the Siberian Synchrotron and Terahertz Radiation Center’s Shared Resource Center. Analytical data on the initial frozen and processed solid samples demonstrate the good repeatability of the results. Quantitative estimates of the sedimentation regimes are obtained, and geochemical indicators of the change in redox conditions are determined from the analysis data. Lithological and geochemical records are synchronized with regional seasonal and annual variations in weather and climate, and with the hydrological regime of the lake for the last 50 years.

Bulletin of the Russian Academy of Sciences: Physics. 2019;83(2):198-203
pages 198-203 views

Upgrade of the Superconducting Multipole Wiggler Magnetic System for the ELETTRA Storage Ring

Khrushchev S.V., Shkaruba V.A., Mezentsev N.A., Tsukanov V.M., Tarasenko O.A., Volkov A.A., Bragin A.V., Lev V.K., Safronov A.N., Karantzoulis E., Zangrando D.

Abstract

The article describes the magnetic system modernization of the wiggler installed at the ELETTRA storage ring in 2002. This work was made in Budker Institute of Nuclear Physycs SB RAS in 2017. Modernization touched, mainly, changes in the parameters of superconducting coils.

Bulletin of the Russian Academy of Sciences: Physics. 2019;83(2):204-207
pages 204-207 views

The 22-Pole Superconducting 7-Tesla Wiggler for the DELTA Storage Ring

Gusev Y.A., Khan S., Khrushchev S.V., Lev V.K., Mezentsev N.A., Safronov A.N., Shkaruba V.A., Tarasenko O.A., Tsukanov V.M., Vasichev S.S., Volkov A.A., Zorin A.V., Bragin A.V., Erokhin A.I.

Abstract

A superconducting wiggler with a magnetic field of 7 T is installed as an insertion device for three X-ray beamlines with photon energies of more than 30 keV used at the Dortmund Electron Accelerator (DELTA, Germany), a source of 1.5 GeV synchrotron radiation. Each of the two side beamlines is separated from the central one by 15 mrad and all three beamlines use a horizontal aperture of 5 mrad. To meet these requirements, the insertion device must have a period of 127 mm and a magnetic field of 7 T for the vertical aperture of a beam vacuum chamber 10 mm long and a flange-to-flange distance of 2.2 m. A superconducting 22-pole wiggler with a field of 7 T and a period of 127 mm operating in the zero boil-off mode is described. The concept and main approaches to designing the magnetic and the cryogenic systems are presented, along with the main parameters and results from testing the new 7-tesla superconducting wiggler for the DELTA storage ring.

Bulletin of the Russian Academy of Sciences: Physics. 2019;83(2):208-214
pages 208-214 views

Сoupled-Mode Equations for the Acousto-Optic Diffraction of a Divergent Beam in an Absorbing Medium

Nikitin P.A.

Abstract

Acousto-optic (AO) interaction in optically isotropic media is studied. Vector differential equations are obtained that describe the Raman–Nath diffraction of light on ultrasound in an absorbing medium. Particular emphasis is placed upon light-beam divergency caused by its transverse restriction.

Bulletin of the Russian Academy of Sciences: Physics. 2019;83(2):215-219
pages 215-219 views

Upgrading a Detector for Studying Fast Processes on a Beam of Synchrotron Radiation

Shekhtman L.I., Aulchenko V.M., Zhulanov V.V., Kudashkin D.V.

Abstract

The current stage of the upgrade of the DIMEX detector for studying fast processes on a synchrotron radiation (SR) beam is described. The current version of the DIMEX is a one-dimensional high-pressure ionization chamber with a fast electron component readout. The detector can record photon fluxes from each bunch separately without mixing photons from different bunches. The maximum flux the DIMEX can detect is limited by the space charge of positive ions in a high-pressure gas. To substantially improve this and other parameters of the detector, it was decided to switch to microstrip silicon technology. A prototype based on a silicon-microstrip sensor was developed along with a special integrated circuit (ASIC) for reading out the signals from this prototype. The first tests of the new DIMEX-Si prototype on an SR beam show that it is superior to the gaseous version in all respects. Results are presented from the first tests of the silicon-microstrip detector prototype on the SR beam of the VEPP-4M storage ring.

Bulletin of the Russian Academy of Sciences: Physics. 2019;83(2):220-224
pages 220-224 views

Experimental Study of Radiation-Induced Evaporation of Cesium Iodide on VEPP-3 Synchrotron Radiation Source

Lemzyakov A.G., Lyakh V.V., Goldenberg B.G., Nazmov V.P., Kozyrev E.A.

Abstract

The thickness and structure of scintillation screens are of paramount importance in X-ray microscopy. A scintillator should be fairly thick in order to maximize the conversion of X-ray quanta to the visible range. At the same time, scattering of light in scintillators considerably reduces the spatial resolution of X-ray images. To improve resolution, the CsI:Tl layer can be structured as a matrix of micropixels to inhibit the spread of light to neighboring cells. In this work, radiation-induced ablation of CsI:Tl with the use of synchrotron radiation is examined as a new way of structuring for scintillation screens.

Bulletin of the Russian Academy of Sciences: Physics. 2019;83(2):225-227
pages 225-227 views

The Novosibirsk Free-Electron Laser Facility

Shevchenko O.A., Vinokurov N.A., Arbuzov V.S., Chernov K.N., Davidyuk I.V., Deichuly O.I., Dementyev E.N., Dovzhenko B.A., Getmanov Y.V., Gorbachev Y.I., Knyazev B.A., Kolobanov E.I., Kondakov A.A., Kozak V.R., Kozyrev E.V., Krutikhin S.A., Kubarev V.V., Kulipanov G.N., Kuper E.A., Kuptsov I.V., Kurkin G.Y., Medvedev L.E., Motygin S.V., Ovchar V.K., Osipov V.N., Petrov V.M., Pilan A.M., Popik V.M., Repkov V.V., Salikova T.V., Scheglov M.A., Sedlyarov I.K., Serednyakov S.S., Skrinsky A.N., Tararyshkin S.V., Tribendis A.G., Tcheskidov V.G., Vobly P.D., Volkov V.N.

Abstract

The Novosibirsk FEL facility has three FELs installed on the first, second, and fourth orbits of the multiturn energy recovery linac (ERL). The first FEL covers the 90–240 μm range of wavelengths at an average radiation power of 0.5 kW with a pulse repetition rate of 5.6 or 11.2 MHz and a peak power of 1 MW. The second FEL operates in the 40–80 μm range of wavelengths at an average radiation power of 0.5 kW with a pulse-repetition rate of 7.5 MHz and a peak power of around 1 MW. These two FELs are the world’s most powerful (in terms of average power) sources of coherent narrow-band (less than 1%) radiation in their wavelength ranges. The third FEL was commissioned in 2015 to cover the 5–20 μm range of wavelengths. The Novosibirsk ERL is the world’s first and only multiturn ERL. Its distinctive features include a normally-conductive 180 MHz accelerating system, a direct current (DC) electrostatic electron gun with a control grid and thermionic cathode, three operating modes of the magnetic system, and a compact (6 × 40 m) design. The Novosibirsk FEL facility has been in operation for users of terahertz radiation since 2004.

Bulletin of the Russian Academy of Sciences: Physics. 2019;83(2):228-231
pages 228-231 views

Morphological Changes in Mammal Skeletal Muscle under the Action of Powerful THz Laser Radiation

Zelentsov E.L., Sazhina T.V., Kozlov A.S., Petrov A.K., Shevchenko O.A.

Abstract

A study is made of morphological changes that occur in the M. Wistar skeletal muscles as a result of tissue damage by focused radiation of the first stage of the Novosibirsk free electron laser. Samples are studied via optical and electron microscopy. The aim of the study is to determine the impact of powerful terahertz radiation and the damage to tissue, compared to CO2 laser radiation. A detailed morphological description and possible causes of tissue damage are given.

Bulletin of the Russian Academy of Sciences: Physics. 2019;83(2):232-236
pages 232-236 views