Application of high-performance liquid chromatography/high-resolution mass spectrometry to the investigation of sodium 2,3-disulfanyl-1-propanesulfonate (unithiol) and products of its oxidation with hydrogen peroxide


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High-performance liquid chromatography combined with high-resolution mass spectrometry has been used to study the mild oxidation of sodium 2,3-disulfanyl-1-propanesulfonate (unithiol) with hydrogen peroxide. Reference peaks have been identified for the initial substance and reaction products. A possibility of using high-performance liquid chromatography with high-resolution mass spectrometry for the Sokolovskii thiol–disulphide test has been shown.

作者简介

D. Kuleshov

Institute for Analytical Instrumentation; St. Petersburg Scientific Center

编辑信件的主要联系方式.
Email: hellchemist@yandex.ru
俄罗斯联邦, St. Petersburg, 198095; St. Petersburg, 199034

T. Berezkina

Ioffe Institute; St. Petersburg Scientific Center

Email: hellchemist@yandex.ru
俄罗斯联邦, St. Petersburg, 194021; St. Petersburg, 199034

Y. Russkikh

St. Petersburg Research Center of Ecological Safety; St. Petersburg Scientific Center

Email: hellchemist@yandex.ru
俄罗斯联邦, St. Petersburg, 197110; St. Petersburg, 199034

E. Chernova

St. Petersburg Research Center of Ecological Safety; St. Petersburg Scientific Center

Email: hellchemist@yandex.ru
俄罗斯联邦, St. Petersburg, 197110; St. Petersburg, 199034

Z. Zhakovskaya

St. Petersburg Research Center of Ecological Safety

Email: hellchemist@yandex.ru
俄罗斯联邦, St. Petersburg, 197110

S. Masyukevich

Institute for Analytical Instrumentation

Email: hellchemist@yandex.ru
俄罗斯联邦, St. Petersburg, 198095

L. Gall

Institute for Analytical Instrumentation; St. Petersburg Scientific Center

Email: hellchemist@yandex.ru
俄罗斯联邦, St. Petersburg, 198095; St. Petersburg, 199034

N. Gall

Institute for Analytical Instrumentation; Ioffe Institute

Email: hellchemist@yandex.ru
俄罗斯联邦, St. Petersburg, 198095; St. Petersburg, 194021


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