Email this article Application of high-performance liquid chromatography/high-resolution mass spectrometry to the investigation of sodium 2,3-disulfanyl-1-propanesulfonate (unithiol) and products of its oxidation with hydrogen peroxide
- Authors: Kuleshov D.O.1,2, Berezkina T.E.3,2, Russkikh Y.V.4,2, Chernova E.N.4,2, Zhakovskaya Z.A.4, Masyukevich S.V.1, Gall L.N.1,2, Gall N.R.1,3
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Affiliations:
- Institute for Analytical Instrumentation
- St. Petersburg Scientific Center
- Ioffe Institute
- St. Petersburg Research Center of Ecological Safety
- Issue: Vol 71, No 14 (2016)
- Pages: 1381-1388
- Section: Articles
- URL: https://journals.rcsi.science/1061-9348/article/view/182256
- DOI: https://doi.org/10.1134/S1061934816140082
- ID: 182256
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Abstract
High-performance liquid chromatography combined with high-resolution mass spectrometry has been used to study the mild oxidation of sodium 2,3-disulfanyl-1-propanesulfonate (unithiol) with hydrogen peroxide. Reference peaks have been identified for the initial substance and reaction products. A possibility of using high-performance liquid chromatography with high-resolution mass spectrometry for the Sokolovskii thiol–disulphide test has been shown.
About the authors
D. O. Kuleshov
Institute for Analytical Instrumentation; St. Petersburg Scientific Center
Author for correspondence.
Email: hellchemist@yandex.ru
Russian Federation, St. Petersburg, 198095; St. Petersburg, 199034
T. E. Berezkina
Ioffe Institute; St. Petersburg Scientific Center
Email: hellchemist@yandex.ru
Russian Federation, St. Petersburg, 194021; St. Petersburg, 199034
Y. V. Russkikh
St. Petersburg Research Center of Ecological Safety; St. Petersburg Scientific Center
Email: hellchemist@yandex.ru
Russian Federation, St. Petersburg, 197110; St. Petersburg, 199034
E. N. Chernova
St. Petersburg Research Center of Ecological Safety; St. Petersburg Scientific Center
Email: hellchemist@yandex.ru
Russian Federation, St. Petersburg, 197110; St. Petersburg, 199034
Z. A. Zhakovskaya
St. Petersburg Research Center of Ecological Safety
Email: hellchemist@yandex.ru
Russian Federation, St. Petersburg, 197110
S. V. Masyukevich
Institute for Analytical Instrumentation
Email: hellchemist@yandex.ru
Russian Federation, St. Petersburg, 198095
L. N. Gall
Institute for Analytical Instrumentation; St. Petersburg Scientific Center
Email: hellchemist@yandex.ru
Russian Federation, St. Petersburg, 198095; St. Petersburg, 199034
N. R. Gall
Institute for Analytical Instrumentation; Ioffe Institute
Email: hellchemist@yandex.ru
Russian Federation, St. Petersburg, 198095; St. Petersburg, 194021
