Determination of boron in organic compounds by microwave plasma–atomic emission spectrometry
- 作者: Bazhenov M.1,2, Tikhova V.1, Fadeeva V.1,2
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隶属关系:
- Novosibirsk Institute of Organic Chemistry
- Novosibirsk National Research State University
- 期: 卷 71, 编号 11 (2016)
- 页面: 1089-1095
- 栏目: Articles
- URL: https://journals.rcsi.science/1061-9348/article/view/182143
- DOI: https://doi.org/10.1134/S1061934816090033
- ID: 182143
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详细
We propose a method for the determination of boron in aliphatic and aromatic trifluoroborates (including perfluorinated ones), ethers, and organoboron compounds containing dioxoborolane fragments, pyridine, and pyrazole rings, and triple bonds. The substances were decomposed by the oxygen flask combustion method. Boron was determined on an Agilent 4100 microwave plasma–atomic emission spectrometer. A number of organic compounds were analyzed, and the mass fraction of boron was determined with an error less than ±0.3 abs. %.
作者简介
M. Bazhenov
Novosibirsk Institute of Organic Chemistry; Novosibirsk National Research State University
Email: tikhova@nioch.nsc.ru
俄罗斯联邦, Novosibirsk, 630090; Novosibirsk, 630090
V. Tikhova
Novosibirsk Institute of Organic Chemistry
编辑信件的主要联系方式.
Email: tikhova@nioch.nsc.ru
俄罗斯联邦, Novosibirsk, 630090
V. Fadeeva
Novosibirsk Institute of Organic Chemistry; Novosibirsk National Research State University
Email: tikhova@nioch.nsc.ru
俄罗斯联邦, Novosibirsk, 630090; Novosibirsk, 630090