Determination of boron in organic compounds by microwave plasma–atomic emission spectrometry
- Authors: Bazhenov M.A.1,2, Tikhova V.D.1, Fadeeva V.P.1,2
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Affiliations:
- Novosibirsk Institute of Organic Chemistry
- Novosibirsk National Research State University
- Issue: Vol 71, No 11 (2016)
- Pages: 1089-1095
- Section: Articles
- URL: https://journals.rcsi.science/1061-9348/article/view/182143
- DOI: https://doi.org/10.1134/S1061934816090033
- ID: 182143
Cite item
Abstract
We propose a method for the determination of boron in aliphatic and aromatic trifluoroborates (including perfluorinated ones), ethers, and organoboron compounds containing dioxoborolane fragments, pyridine, and pyrazole rings, and triple bonds. The substances were decomposed by the oxygen flask combustion method. Boron was determined on an Agilent 4100 microwave plasma–atomic emission spectrometer. A number of organic compounds were analyzed, and the mass fraction of boron was determined with an error less than ±0.3 abs. %.
About the authors
M. A. Bazhenov
Novosibirsk Institute of Organic Chemistry; Novosibirsk National Research State University
Email: tikhova@nioch.nsc.ru
Russian Federation, Novosibirsk, 630090; Novosibirsk, 630090
V. D. Tikhova
Novosibirsk Institute of Organic Chemistry
Author for correspondence.
Email: tikhova@nioch.nsc.ru
Russian Federation, Novosibirsk, 630090
V. P. Fadeeva
Novosibirsk Institute of Organic Chemistry; Novosibirsk National Research State University
Email: tikhova@nioch.nsc.ru
Russian Federation, Novosibirsk, 630090; Novosibirsk, 630090