Email this article The Method for Determining the Exact Single Crystal Orientation with Simultaneous X-Ray Energy Correction Using the Spectrum of Diffraction Losses
- Authors: Klimova N.B.1, Snigirev A.A.1
-
Affiliations:
- Immanuel Kant Baltic Federal University
- Issue: No 10 (2023)
- Pages: 59-68
- Section: Articles
- URL: https://journals.rcsi.science/1028-0960/article/view/141028
- DOI: https://doi.org/10.31857/S1028096023100084
- EDN: https://elibrary.ru/LAFKWU
- ID: 141028
Cite item
Open Access
Access granted
Subscription Access
Abstract
The intensity loss of transmitted beam due to parasitic diffraction (glitches) is an inherent property of single-crystal X-ray optics. This effect can lead to a weakening of the radiation, up to its complete disappearance. Therefore, understanding the effect of diffraction loss is essential for any experiments that use single-crystal optics. We present theory of glitch formation and demonstrate its application to experimental data to determine the orientation and cell parameters of optical elements made of the single-crystal diamond. A systematic error was found in determining the absolute energy of X-ray, which occurs due to the wrong monochromator tuning (an error in determining the absolute 2θ angle). The described error very often occurs during the experiment as a result of the fact that determining the absolute 2θ angle of the monochromator crystal is a technically difficult task. Simultaneous determination of the orientation and lattice parameters of the studied sample, together with the compensation of the systematic error in the monochromator tuning, made it possible to significantly improve the accuracy of processing the obtained data.
About the authors
N. B. Klimova
Immanuel Kant Baltic Federal University
Author for correspondence.
Email: klimovanb@gmail.com
Russia, 236014, Kaliningrad
A. A. Snigirev
Immanuel Kant Baltic Federal University
Author for correspondence.
Email: anatoly.snigirev@gmail.com
Russia, 236014, Kaliningrad
References
- Dobson B.R., Hasnain S.S., Morrell C., Konigsberger D.C., Pandya K., Kampers F., Van Zuylen P., Van Der Hoek M.J. // Rev. Sci. Instrum. 1989. V. 60. P. 2511. https://doi.org/10.1063/1.1140715
- Rowen M., Wong J., Tanaka T. // J. Phys. IV France. 1997. V. 7. P. C2. https://doi.org/10.1051/jp4/1997208
- Polikarpov M., Emerich H., Klimova N., Snigireva I., Savin V., Snigirev A. // Phys. Stat. Sol. B. 2018. V. 255. P. 1700229. https://doi.org/10.1002/pssb.201700229
- Zhang Q., Polikarpov M., Klimova N., Larsen H.B., Mathiesen R., Emerich H., Thorkildsen G., Snigireva I., Snigirev A. // J. Synchrotron Radiat. 2019. V. 26. № 1. P. 109. https://doi.org/10.1107/S1600577518014856
- Bauchspiess K.R., Crozier E.D. // EXAFS and Near Edge Structure III. Springer Proceedings in Physics. V. 2 / Ed. Hodgson K.O., Hedman B., Penner-Hahn J.E. Berlin–Heidelberg: Springer, 1984. P. 514. https://doi.org/10.1007/978-3-642-46522-2
- Van Zuylen P., Van Der Hoek M.J. // Proc. SPIE. 1986. V. 0733. P. 248. https://doi.org/10.1117/12.964917
- Van Der Laan G., Thole B.T // Nucl. Instrum. Methods Phys. Res. A. 1988. V. 263. P. 515. https://doi.org/10.1016/0168-9002(88)90995-3
- Kononenko T.V., Ralchenko V.G., Ashkinazi E.E., Polikarpov M., Ershov P., Kuznetsov S., Yunkin V., Snigireva I., Konov V.I. // Appl. Phys. A. 2016. V. 122. P. 1. https://doi.org/10.1007/s00339-016-9683-9
- Tang Z., Zheng L., Chu S., Wu M., An P., Zhang L., Hu T. // J. Synchrotron Radiat. 2015. V. 22. P. 1147. https://doi.org/10.1107/S1600577515012345
- Monochromator Crystal Glitch Library. Available online: https://www-ssrl.slac.stanford.edu/~xas/glitch/ glitch.html (accessed on 16 March 2021).
- Samuel M., Wallace, Marco A.A., Gaillard J.-F. An Algorithm for the Automatic Deglitching of X-Ray Absorption Spectroscopy Data. License CC BY-SA 4.0 2020.
- Sutter J.P., Boada R., Bowron D.T., Stepanov S.A., Díaz-Moreno S. // J. Appl. Crystallogr. 2016. V. 49. P. 4. P. 1209. https://doi.org/10.1107/S1600576716009183
- Abe H., Aquilanti G., Boada R., Bunker B., Glatzel P., Nachtegaal M., Pascarelli S. // J. Synchrotron Radiat. 2018. V. 25. P. 972. https://doi.org/10.1107/S1600577518006021
- Klimova N., Yefanov O., Snigirev A. // AIP Conf. Proc. 2020. V. 2299. P. 060016. https://doi.org/10.1063/5.0030507
- Klimova N., Yefanov O., Snigireva I., Snigirev A. // Crystals. 2021. V. 11. № 5. P. 504. https://doi.org/10.3390/cryst11050504
- Klimova N., Snigireva I., Snigirev A., Yefanov O. // Crystals. 2021. V. 11. № 12. P. 1561. https://doi.org/10.3390/cryst11121561
- Klimova N., Snigireva I., Snigirev A., Yefanov O. // J. Synchrotron Radiat. 2022. V. 29. P. 369. https://doi.org/10.1107/S1600577521013667
- Программы для расчета глитчей в монокристаллической рентгеновской оптике: https://github.com/ XrayViz/Glitches.
- Yefanov O., Kladko V., Slobodyan M., Polischuk Y. // J. Appl. Crystallogr. 2008. V. 41. P. 647. https://doi.org/10.1107/S0021889808008625
- Authier A. // Dynamical Theory of X-Ray Diffraction. Oxford University Press, 2003. P. 661. https://doi.org/10.1093/acprof:oso/9780198528920. 001.0001
- Snigirev A., Kohn V., Snigireva I., Lengeler B. // Nature. 1996. V. 384. № 6604. P. 49. https://doi.org/10.1038/384049a0
- Schroer C.G., Lengler B., Benner B., Kuhlmann M., Guenzler T.F., Tuemmler J., Rau C., Weitkamp T., Snigirev A., Snigireva I. // Proc. SPIE. 2001. V. 4145. P. 274. https://doi.org/10.1117/12.411647
- Polikarpov M., Snigireva I., Morse J., Yunkin V., Kuznetsov S., Snigirev A. // J. Synchrotron Radiat. 2015. V. 22. P. 23. https://doi.org/10.1107/S1600577514021742
- Micro Usinage Laser. Available online: http://micro-usinage-laser.com/ (accessed on 16 March 2021).
- New Diamond Technology. Available online: http:// ndtcompany.com/ (accessed on 16 March 2021).
- Element Six Ltd. Available online: https://www.e6.com/ (accessed on 16 March 2021).
- Terentyev S., Blank V., Polyakov S., Zholudev S., Snigirev A., Polikarpov M., Kolodziej T., Qian J., Zhou H., Shvyd’ko Y. // Appl. Phys. Lett. 2015. V. 107. P. 111108. https://doi.org/10.1063/1.4931357
Supplementary files
