Validation of a GC-MS Method for Quantitative Determination of Cyclohexanone by Oxidative Cleavage
- 作者: Podrezova E.1, Lar’kina M.2, Yusubov M.1,2, Belousov M.2, Zamanova M.1, Krivoshchekov S.1,2
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隶属关系:
- Tomsk State Polytechnic University
- Siberian State Medical University
- 期: 卷 52, 编号 12 (2019)
- 页面: 1021-1025
- 栏目: Article
- URL: https://journals.rcsi.science/0091-150X/article/view/245586
- DOI: https://doi.org/10.1007/s11094-019-01945-w
- ID: 245586
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详细
A GC method for quantitative determination of cyclohexanone by oxidative cleavage was proposed. The research was aimed at the development of a simple, rapid, and effective GC method for quantitative analysis of cyclohexanone in a reaction mixture. Chlorobenzene was used as an internal standard. Qualitative analysis compared mass spectra obtained for each component with mass spectra from the National Institute of Standards and Technology (NIST) database. The method was validated for specificity, linearity, accuracy, robustness, repeatability, and intralaboratory precision.
作者简介
E. Podrezova
Tomsk State Polytechnic University
Email: marialarkina@mail.ru
俄罗斯联邦, 30 Prosp. Lenina, Tomsk, 634050
M. Lar’kina
Siberian State Medical University
编辑信件的主要联系方式.
Email: marialarkina@mail.ru
俄罗斯联邦, 2 Moskovskii Trakt, Tomsk, 634040
M. Yusubov
Tomsk State Polytechnic University; Siberian State Medical University
Email: marialarkina@mail.ru
俄罗斯联邦, 30 Prosp. Lenina, Tomsk, 634050; 2 Moskovskii Trakt, Tomsk, 634040
M. Belousov
Siberian State Medical University
Email: marialarkina@mail.ru
俄罗斯联邦, 2 Moskovskii Trakt, Tomsk, 634040
M. Zamanova
Tomsk State Polytechnic University
Email: marialarkina@mail.ru
俄罗斯联邦, 30 Prosp. Lenina, Tomsk, 634050
S. Krivoshchekov
Tomsk State Polytechnic University; Siberian State Medical University
Email: marialarkina@mail.ru
俄罗斯联邦, 30 Prosp. Lenina, Tomsk, 634050; 2 Moskovskii Trakt, Tomsk, 634040