Validation of a GC-MS Method for Quantitative Determination of Cyclohexanone by Oxidative Cleavage
- Авторлар: Podrezova E.1, Lar’kina M.2, Yusubov M.1,2, Belousov M.2, Zamanova M.1, Krivoshchekov S.1,2
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Мекемелер:
- Tomsk State Polytechnic University
- Siberian State Medical University
- Шығарылым: Том 52, № 12 (2019)
- Беттер: 1021-1025
- Бөлім: Article
- URL: https://journals.rcsi.science/0091-150X/article/view/245586
- DOI: https://doi.org/10.1007/s11094-019-01945-w
- ID: 245586
Дәйексөз келтіру
Аннотация
A GC method for quantitative determination of cyclohexanone by oxidative cleavage was proposed. The research was aimed at the development of a simple, rapid, and effective GC method for quantitative analysis of cyclohexanone in a reaction mixture. Chlorobenzene was used as an internal standard. Qualitative analysis compared mass spectra obtained for each component with mass spectra from the National Institute of Standards and Technology (NIST) database. The method was validated for specificity, linearity, accuracy, robustness, repeatability, and intralaboratory precision.
Авторлар туралы
E. Podrezova
Tomsk State Polytechnic University
Email: marialarkina@mail.ru
Ресей, 30 Prosp. Lenina, Tomsk, 634050
M. Lar’kina
Siberian State Medical University
Хат алмасуға жауапты Автор.
Email: marialarkina@mail.ru
Ресей, 2 Moskovskii Trakt, Tomsk, 634040
M. Yusubov
Tomsk State Polytechnic University; Siberian State Medical University
Email: marialarkina@mail.ru
Ресей, 30 Prosp. Lenina, Tomsk, 634050; 2 Moskovskii Trakt, Tomsk, 634040
M. Belousov
Siberian State Medical University
Email: marialarkina@mail.ru
Ресей, 2 Moskovskii Trakt, Tomsk, 634040
M. Zamanova
Tomsk State Polytechnic University
Email: marialarkina@mail.ru
Ресей, 30 Prosp. Lenina, Tomsk, 634050
S. Krivoshchekov
Tomsk State Polytechnic University; Siberian State Medical University
Email: marialarkina@mail.ru
Ресей, 30 Prosp. Lenina, Tomsk, 634050; 2 Moskovskii Trakt, Tomsk, 634040