Validation of a GC-MS Method for Quantitative Determination of Cyclohexanone by Oxidative Cleavage
- Autores: Podrezova E.1, Lar’kina M.2, Yusubov M.1,2, Belousov M.2, Zamanova M.1, Krivoshchekov S.1,2
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Afiliações:
- Tomsk State Polytechnic University
- Siberian State Medical University
- Edição: Volume 52, Nº 12 (2019)
- Páginas: 1021-1025
- Seção: Article
- URL: https://journals.rcsi.science/0091-150X/article/view/245586
- DOI: https://doi.org/10.1007/s11094-019-01945-w
- ID: 245586
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Resumo
A GC method for quantitative determination of cyclohexanone by oxidative cleavage was proposed. The research was aimed at the development of a simple, rapid, and effective GC method for quantitative analysis of cyclohexanone in a reaction mixture. Chlorobenzene was used as an internal standard. Qualitative analysis compared mass spectra obtained for each component with mass spectra from the National Institute of Standards and Technology (NIST) database. The method was validated for specificity, linearity, accuracy, robustness, repeatability, and intralaboratory precision.
Sobre autores
E. Podrezova
Tomsk State Polytechnic University
Email: marialarkina@mail.ru
Rússia, 30 Prosp. Lenina, Tomsk, 634050
M. Lar’kina
Siberian State Medical University
Autor responsável pela correspondência
Email: marialarkina@mail.ru
Rússia, 2 Moskovskii Trakt, Tomsk, 634040
M. Yusubov
Tomsk State Polytechnic University; Siberian State Medical University
Email: marialarkina@mail.ru
Rússia, 30 Prosp. Lenina, Tomsk, 634050; 2 Moskovskii Trakt, Tomsk, 634040
M. Belousov
Siberian State Medical University
Email: marialarkina@mail.ru
Rússia, 2 Moskovskii Trakt, Tomsk, 634040
M. Zamanova
Tomsk State Polytechnic University
Email: marialarkina@mail.ru
Rússia, 30 Prosp. Lenina, Tomsk, 634050
S. Krivoshchekov
Tomsk State Polytechnic University; Siberian State Medical University
Email: marialarkina@mail.ru
Rússia, 30 Prosp. Lenina, Tomsk, 634050; 2 Moskovskii Trakt, Tomsk, 634040