Synthesis and Elucidation of Structure of Deuterated Androsta-3,5-diene-7,17-dione


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The title compound was synthesized as an internal standard for the quantitative determination of Arimistane in biological samples. [2H7] Arimistane was obtained from Arimistane-d0 by alkaline H/2H exchange of the С2,4,6,8,16 protons. The location of the labels was confirmed by NMR spectroscopy. The spatial structures were studied by X-ray diffraction.

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V. Abzianidze

Chemical Modeling Laboratory, Research Institute of Hygiene, Occupational Pathology and Human Ecology

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Email: vvaavv@mail.ru
俄罗斯联邦, p/o Kuz’molovsky, St. Petersburg, 188663

T. Panikorovskii

Department of Crystallography, Institute of Earth Sciences

Email: vvaavv@mail.ru
俄罗斯联邦, Universitetskaya nab.7–9, St. Petersburg, 199034

L. Chisty

Chemical Modeling Laboratory, Research Institute of Hygiene, Occupational Pathology and Human Ecology

Email: vvaavv@mail.ru
俄罗斯联邦, p/o Kuz’molovsky, St. Petersburg, 188663

D. Kochura

Chemical Modeling Laboratory, Research Institute of Hygiene, Occupational Pathology and Human Ecology

Email: vvaavv@mail.ru
俄罗斯联邦, p/o Kuz’molovsky, St. Petersburg, 188663

D. Krivorotov

Chemical Modeling Laboratory, Research Institute of Hygiene, Occupational Pathology and Human Ecology

Email: vvaavv@mail.ru
俄罗斯联邦, p/o Kuz’molovsky, St. Petersburg, 188663

V. Kuznetsov

Chemical Modeling Laboratory, Research Institute of Hygiene, Occupational Pathology and Human Ecology

Email: vvaavv@mail.ru
俄罗斯联邦, p/o Kuz’molovsky, St. Petersburg, 188663

A. Radilov

Chemical Modeling Laboratory, Research Institute of Hygiene, Occupational Pathology and Human Ecology

Email: vvaavv@mail.ru
俄罗斯联邦, p/o Kuz’molovsky, St. Petersburg, 188663


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