Synthesis and Elucidation of Structure of Deuterated Androsta-3,5-diene-7,17-dione

V. V. Abzianidze; T. L. Panikorovskii; L. S. Chisty; D. M. Kochura; D. V. Krivorotov; V. A. Kuznetsov; A. S. Radilov

doi:10.1134/S1070363217120520

Synthesis and Elucidation of Structure of Deuterated Androsta-3,5-diene-7,17-dione

Авторы: Abzianidze V.¹, Panikorovskii T.², Chisty L.¹, Kochura D.¹, Krivorotov D.¹, Kuznetsov V.¹, Radilov A.¹
Учреждения:
1. Chemical Modeling Laboratory, Research Institute of Hygiene, Occupational Pathology and Human Ecology
2. Department of Crystallography, Institute of Earth Sciences
Выпуск: Том 87, № 12 (2017)
Страницы: 3052-3058
Раздел: Letters to the Editor
URL: https://journals.rcsi.science/1070-3632/article/view/221860
DOI: https://doi.org/10.1134/S1070363217120520
ID: 221860

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Аннотация
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Аннотация

The title compound was synthesized as an internal standard for the quantitative determination of Arimistane in biological samples. [²H₇] Arimistane was obtained from Arimistane-d₀ by alkaline H/²H exchange of the С^2,4,6,8,16 protons. The location of the labels was confirmed by NMR spectroscopy. The spatial structures were studied by X-ray diffraction.