Email this article Synthesis and Characterization of Barium Amidoborane
- Authors: Shcherbina N.A.1, Kazakov I.V.1, Timoshkin A.Y.1
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Affiliations:
- St. Petersburg State University
- Issue: Vol 87, No 12 (2017)
- Pages: 2875-2877
- Section: Letters to the Editor
- URL: https://journals.rcsi.science/1070-3632/article/view/221717
- DOI: https://doi.org/10.1134/S1070363217120192
- ID: 221717
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Abstract
Barium amidoborane was synthesized for the first time by the reaction of metal barium with ammonia borane. The compound was characterized by the methods of the solid-phase 11B NMR and IR spectroscopy and elemental analysis. It was shown by simultaneous thermal analysis that hydrogen is the only volatile product of barium amidoborane decomposition in the temperature range 50–240°C.
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About the authors
N. A. Shcherbina
St. Petersburg State University
Email: a.y.timoshkin@spbu.ru
Russian Federation, Universitetskii pr. 26, St. Petersburg, 198504
I. V. Kazakov
St. Petersburg State University
Email: a.y.timoshkin@spbu.ru
Russian Federation, Universitetskii pr. 26, St. Petersburg, 198504
A. Yu. Timoshkin
St. Petersburg State University
Author for correspondence.
Email: a.y.timoshkin@spbu.ru
Russian Federation, Universitetskii pr. 26, St. Petersburg, 198504
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