Synthesis of Bisthiacalix[4]arene: Reaction of Piperazine with Monoacrylamide Derivative of p-tert-Butylthiacalix[4]arene
- Autores: Nosov R.1, Stoikov I.1
-
Afiliações:
- Butlerov Chemical Institute
- Edição: Volume 88, Nº 11 (2018)
- Páginas: 2314-2320
- Seção: Article
- URL: https://journals.rcsi.science/1070-3632/article/view/222532
- DOI: https://doi.org/10.1134/S1070363218110117
- ID: 222532
Citar
Resumo
The reaction of acryloyl chloride with the monoamine derivative of p-tert-butylthiacalix[4]arene was used to synthesize p-tert-butylthiacalix[4]arene monoacrylamide in the 1,3-alternate conformation. The effect of the nature of the amine on the result of its Michael reaction with the synthesized p-tert-butylthiacalix[4]arene monoacrylamide was studied. The latter was reacted with piperazine to obtain bisthiacalix[4]arene with the macrocyclic fragments in the 1,3-alternate conformation.
Palavras-chave
Sobre autores
R. Nosov
Butlerov Chemical Institute
Email: ivan.stoikov@mail.ru
Rússia, ul. Kremlevskaya 18, Kazan, Tatarstan, 420008
I. Stoikov
Butlerov Chemical Institute
Autor responsável pela correspondência
Email: ivan.stoikov@mail.ru
Rússia, ul. Kremlevskaya 18, Kazan, Tatarstan, 420008
![](/img/style/loading.gif)