Multicomponent cyclothiomethylation of phenylenediamines and 4,4'-diaminodiphenyls with formaldehyde and 1,2-ethanedithiol
- Autores: Khabibullina G.1, Fedotova E.1, Anpilogova G.2, Akhmetova V.1, Ibragimov A.1
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Afiliações:
- Institute of Petrochemistry and Catalysis
- Ufa Institute of Chemistry
- Edição: Volume 86, Nº 7 (2016)
- Páginas: 1608-1612
- Seção: Article
- URL: https://journals.rcsi.science/1070-3632/article/view/215656
- DOI: https://doi.org/10.1134/S1070363216070124
- ID: 215656
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Resumo
One-pot synthesis of bis-1,5,3-dithiazepanes by cyclothiomethylation of o-phenylenediamine, 4,4'-diaminodiphenyl, 4,4'-diaminodiphenyl oxide, and 4,4'-diaminodiphenylmethane with formaldehyde and 1,2- ethanedithiol was performed. Sorption properties of the newly synthesized bis[4-(1,5,3-dithiazepan-3-yl)-phenyl] oxide were investigated by the batch technique. High efficiency of the recovery of palladium(II) with this reagent from hydrochloric acid solutions at room temperature was shown.
Sobre autores
G. Khabibullina
Institute of Petrochemistry and Catalysis
Autor responsável pela correspondência
Email: ink@anrb.ru
Rússia, pr. Oktyabrya 141, Ufa, 450075
E. Fedotova
Institute of Petrochemistry and Catalysis
Email: ink@anrb.ru
Rússia, pr. Oktyabrya 141, Ufa, 450075
G. Anpilogova
Ufa Institute of Chemistry
Email: ink@anrb.ru
Rússia, Ufa
V. Akhmetova
Institute of Petrochemistry and Catalysis
Email: ink@anrb.ru
Rússia, pr. Oktyabrya 141, Ufa, 450075
A. Ibragimov
Institute of Petrochemistry and Catalysis
Email: ink@anrb.ru
Rússia, pr. Oktyabrya 141, Ufa, 450075