Disulfide derivatives of thiosemicarbazones of 4-formyl-5-thiopyrazole
- Авторлар: Uraev A.1, Korobov M.1, Popov L.2, Aleksandrov G.3, Korshunova E.1, Garnovskii D.4, Burlov A.1
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Мекемелер:
- Research Institute of Physical and Organic Chemistry
- Chemical Department
- N. S. Kurnakov Institute of General and Inorganic Chemistry
- Southern Scientific Center
- Шығарылым: Том 87, № 2 (2017)
- Беттер: 252-258
- Бөлім: Article
- URL: https://journals.rcsi.science/1070-3632/article/view/218263
- DOI: https://doi.org/10.1134/S1070363217020165
- ID: 218263
Дәйексөз келтіру
Аннотация
The reaction of 4-formyl-5-mercaptopyrazole with thiosemicarbazides in methanol has afforded novel disulfide derivatives of thiosemicarbazones, and their structure has been studied by NMR and IR spectroscopy. X-ray diffraction analysis of [5,5'-dithiobis(4-formyl-3-methyl-1-phenylpyrazole)]-4-allylthio-semicarbazone has shown that it exists as a dimer with two molecules linked via the disulfide S–S bridge between the heterocycles in the crystal.
Негізгі сөздер
Авторлар туралы
A. Uraev
Research Institute of Physical and Organic Chemistry
Хат алмасуға жауапты Автор.
Email: uraevali@yandex.ru
Ресей, pr. Stachki 194/2, Rostov-on-Don, 344090
M. Korobov
Research Institute of Physical and Organic Chemistry
Email: uraevali@yandex.ru
Ресей, pr. Stachki 194/2, Rostov-on-Don, 344090
L. Popov
Chemical Department
Email: uraevali@yandex.ru
Ресей, Rostov-on-Don
G. Aleksandrov
N. S. Kurnakov Institute of General and Inorganic Chemistry
Email: uraevali@yandex.ru
Ресей, Moscow
E. Korshunova
Research Institute of Physical and Organic Chemistry
Email: uraevali@yandex.ru
Ресей, pr. Stachki 194/2, Rostov-on-Don, 344090
D. Garnovskii
Southern Scientific Center
Email: uraevali@yandex.ru
Ресей, Rostov-on-Don
A. Burlov
Research Institute of Physical and Organic Chemistry
Email: uraevali@yandex.ru
Ресей, pr. Stachki 194/2, Rostov-on-Don, 344090
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