Preparation, Characterization, and Application of Preyssler Heteropoly Acid Immobilized on Magnetic Nanoparticles as a Green and Recoverable Catalyst for the Synthesis of Imidazoles
- Authors: Javid A.1, Khojastehnezhad A.2, Pombeiro A.J.3
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Affiliations:
- Department of Chemistry, Ahvaz Branch
- Young Researchers and Elite Club, Mashhad Branch
- Centro de Quimica Estrutural, Instituto Superior Técnico
- Issue: Vol 87, No 12 (2017)
- Pages: 3000-3005
- Section: Letters to the Editor
- URL: https://journals.rcsi.science/1070-3632/article/view/221820
- DOI: https://doi.org/10.1134/S1070363217120453
- ID: 221820
Cite item
Abstract
An efficient, magnetically separable catalyst was synthesized by immobilization of Preyssler heteropoly acid (HPA) on Ni0.5Zn0.5Fe2O4 magnetite nanoparticles (MNPs) coated with hydroxyapatite (HA). The catalyst was characterized by scaning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), FT-IR, energy dispersive spectroscopy (EDS), and TGA. Activity of this catalyst was tested in the synthesis of imidazole derivatives via one-pot three-component condensation of [9,10]-phenanthraquinone with aryl aldehydes and ammonium acetate at room temperature under solvent-free conditions.
About the authors
A. Javid
Department of Chemistry, Ahvaz Branch
Author for correspondence.
Email: alijavid@iauahvaz.ac.ir
Iran, Islamic Republic of, Ahvaz
A. Khojastehnezhad
Young Researchers and Elite Club, Mashhad Branch
Email: alijavid@iauahvaz.ac.ir
Iran, Islamic Republic of, Mashhad
A. J. L. Pombeiro
Centro de Quimica Estrutural, Instituto Superior Técnico
Email: alijavid@iauahvaz.ac.ir
Portugal, av. Rovisco Pais, Lisboa, 1049-001
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