Мақаланы E-mail арқылы жіберу Selective synthesis of cyclic triperoxides from 1,1′-dihydroperoxydi(cycloalkyl)peroxides and acetals using SnCl4
- Авторлар: Radulov P.S.1,2, Belyakova Y.Y.1, Demina A.A.3, Nikishin G.I.1, Yaremenko I.A.1,2,4, Terent’ev A.O.1,2,4
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Мекемелер:
- N. D. Zelinsky Institute of Organic Chemistry of the Russian Academy of Sciences
- All-Russia Research Institute for Phytopathology
- M. V. Lomonosov Moscow State University
- D. I. Mendeleev University of Chemical Technology of Russia
- Шығарылым: Том 68, № 6 (2019)
- Беттер: 1289-1292
- Бөлім: Brief Communication
- URL: https://journals.rcsi.science/1066-5285/article/view/243416
- DOI: https://doi.org/10.1007/s11172-019-2555-7
- ID: 243416
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Аннотация
A method for the synthesis of 1,2,4,5,7,8-hexaoxonanes by the reaction of 1,1′-dihydroperoxydi(cycloalkyl)peroxides with acetals using SnCl4 has been developed. For the first time, it was shown that SnCl4 can serve as an effective reagent for the synthesis of cyclic organic peroxides. The proposed method allows obtaining 9-membered cyclic triperoxides selectively and in the yields of up to 90% based on the isolated product.
Авторлар туралы
P. Radulov
N. D. Zelinsky Institute of Organic Chemistry of the Russian Academy of Sciences; All-Russia Research Institute for Phytopathology
Email: terentev@ioc.ac.ru
Ресей, 47 Leninsky prosp., Moscow, 119991; 5 ul. Institut, Bolshie Vyazyomy, Odintsovo District, Moscow Region, 143050
Yu. Belyakova
N. D. Zelinsky Institute of Organic Chemistry of the Russian Academy of Sciences
Email: terentev@ioc.ac.ru
Ресей, 47 Leninsky prosp., Moscow, 119991
A. Demina
M. V. Lomonosov Moscow State University
Email: terentev@ioc.ac.ru
Ресей, 1-3 Leninskiye Gory, Moscow, 119991
G. Nikishin
N. D. Zelinsky Institute of Organic Chemistry of the Russian Academy of Sciences
Email: terentev@ioc.ac.ru
Ресей, 47 Leninsky prosp., Moscow, 119991
I. Yaremenko
N. D. Zelinsky Institute of Organic Chemistry of the Russian Academy of Sciences; All-Russia Research Institute for Phytopathology; D. I. Mendeleev University of Chemical Technology of Russia
Email: terentev@ioc.ac.ru
Ресей, 47 Leninsky prosp., Moscow, 119991; 5 ul. Institut, Bolshie Vyazyomy, Odintsovo District, Moscow Region, 143050; 9 Miusskaya pl., Moscow, 125047
A. Terent’ev
N. D. Zelinsky Institute of Organic Chemistry of the Russian Academy of Sciences; All-Russia Research Institute for Phytopathology; D. I. Mendeleev University of Chemical Technology of Russia
Хат алмасуға жауапты Автор.
Email: terentev@ioc.ac.ru
Ресей, 47 Leninsky prosp., Moscow, 119991; 5 ul. Institut, Bolshie Vyazyomy, Odintsovo District, Moscow Region, 143050; 9 Miusskaya pl., Moscow, 125047
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