电邮这篇文章 Selective synthesis of cyclic triperoxides from 1,1′-dihydroperoxydi(cycloalkyl)peroxides and acetals using SnCl4
- 作者: Radulov P.S.1,2, Belyakova Y.Y.1, Demina A.A.3, Nikishin G.I.1, Yaremenko I.A.1,2,4, Terent’ev A.O.1,2,4
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隶属关系:
- N. D. Zelinsky Institute of Organic Chemistry of the Russian Academy of Sciences
- All-Russia Research Institute for Phytopathology
- M. V. Lomonosov Moscow State University
- D. I. Mendeleev University of Chemical Technology of Russia
- 期: 卷 68, 编号 6 (2019)
- 页面: 1289-1292
- 栏目: Brief Communication
- URL: https://journals.rcsi.science/1066-5285/article/view/243416
- DOI: https://doi.org/10.1007/s11172-019-2555-7
- ID: 243416
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详细
A method for the synthesis of 1,2,4,5,7,8-hexaoxonanes by the reaction of 1,1′-dihydroperoxydi(cycloalkyl)peroxides with acetals using SnCl4 has been developed. For the first time, it was shown that SnCl4 can serve as an effective reagent for the synthesis of cyclic organic peroxides. The proposed method allows obtaining 9-membered cyclic triperoxides selectively and in the yields of up to 90% based on the isolated product.
作者简介
P. Radulov
N. D. Zelinsky Institute of Organic Chemistry of the Russian Academy of Sciences; All-Russia Research Institute for Phytopathology
Email: terentev@ioc.ac.ru
俄罗斯联邦, 47 Leninsky prosp., Moscow, 119991; 5 ul. Institut, Bolshie Vyazyomy, Odintsovo District, Moscow Region, 143050
Yu. Belyakova
N. D. Zelinsky Institute of Organic Chemistry of the Russian Academy of Sciences
Email: terentev@ioc.ac.ru
俄罗斯联邦, 47 Leninsky prosp., Moscow, 119991
A. Demina
M. V. Lomonosov Moscow State University
Email: terentev@ioc.ac.ru
俄罗斯联邦, 1-3 Leninskiye Gory, Moscow, 119991
G. Nikishin
N. D. Zelinsky Institute of Organic Chemistry of the Russian Academy of Sciences
Email: terentev@ioc.ac.ru
俄罗斯联邦, 47 Leninsky prosp., Moscow, 119991
I. Yaremenko
N. D. Zelinsky Institute of Organic Chemistry of the Russian Academy of Sciences; All-Russia Research Institute for Phytopathology; D. I. Mendeleev University of Chemical Technology of Russia
Email: terentev@ioc.ac.ru
俄罗斯联邦, 47 Leninsky prosp., Moscow, 119991; 5 ul. Institut, Bolshie Vyazyomy, Odintsovo District, Moscow Region, 143050; 9 Miusskaya pl., Moscow, 125047
A. Terent’ev
N. D. Zelinsky Institute of Organic Chemistry of the Russian Academy of Sciences; All-Russia Research Institute for Phytopathology; D. I. Mendeleev University of Chemical Technology of Russia
编辑信件的主要联系方式.
Email: terentev@ioc.ac.ru
俄罗斯联邦, 47 Leninsky prosp., Moscow, 119991; 5 ul. Institut, Bolshie Vyazyomy, Odintsovo District, Moscow Region, 143050; 9 Miusskaya pl., Moscow, 125047
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