Synthesis of fluorine-containing esters of 2,5-furandicarboxylic acid

A. M. Sakharov; O. U. Smirnova; A. A. Glazkov; A. A. Yarosh

doi:10.1007/s11172-018-2304-3

Synthesis of fluorine-containing esters of 2,5-furandicarboxylic acid

Authors: Sakharov A.M.¹, Smirnova O.U.¹, Glazkov A.A.¹, Yarosh A.A.¹
Affiliations:
1. N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences
Issue: Vol 67, No 10 (2018)
Pages: 1899-1902
Section: Article
URL: https://journals.rcsi.science/1066-5285/article/view/243113
DOI: https://doi.org/10.1007/s11172-018-2304-3
ID: 243113

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Abstract

Fluorinated esters of 2,5-furandicarboxylic acid have been synthesized starting from 2,5-furan dicarboxylic acid dichloride and fluorine-containing diols. The reaction control was performed by means of ¹H, ¹⁹F NMR, and IR-spectroscopy. Thermal stability, as well as glass transition temperature, and intrinsic viscosity parameters of the obtained oligomers have been determined.