Synthesis of fluorine-containing esters of 2,5-furandicarboxylic acid

A. M. Sakharov; O. U. Smirnova; A. A. Glazkov; A. A. Yarosh

doi:10.1007/s11172-018-2304-3

Synthesis of fluorine-containing esters of 2,5-furandicarboxylic acid

Авторы: Sakharov A.¹, Smirnova O.¹, Glazkov A.¹, Yarosh A.¹
Учреждения:
1. N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences
Выпуск: Том 67, № 10 (2018)
Страницы: 1899-1902
Раздел: Article
URL: https://journals.rcsi.science/1066-5285/article/view/243113
DOI: https://doi.org/10.1007/s11172-018-2304-3
ID: 243113

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Аннотация

Fluorinated esters of 2,5-furandicarboxylic acid have been synthesized starting from 2,5-furan dicarboxylic acid dichloride and fluorine-containing diols. The reaction control was performed by means of ¹H, ¹⁹F NMR, and IR-spectroscopy. Thermal stability, as well as glass transition temperature, and intrinsic viscosity parameters of the obtained oligomers have been determined.