Peculiarities of the Crystal Structure and Texture of Isotropic and Anisotropic Polycrystalline Hexagonal Ferrites BaFe12O19 Synthesized by Radiation-Thermal Sintering
- Authors: Isaev I.M.1, Bryazgin A.A.2, Korobeynikov M.V.2, Mihaylenko M.A.2, Kalinyuk M.V.3, Belokon’ E.A.1,4, Korovushkin V.V.1, Alekseev A.A.1,4, Ostafijchuk B.K.3, Mokljak V.V.5, Nalogin A.G.4, Kostishin V.G.1, Shcherbakov S.V.4, Salogub D.V.1
-
Affiliations:
- National University of Science and Technology MISIS
- Budker Institute of Nuclear Physics, Siberian Branch, Russian Academy of Sciences
- Stefanyk Precarpathian National University
- AO NPP Istok im. Shokina
- Kurdyumov Institute for Metal Physics, National Academy of Sciences
- Issue: Vol 48, No 8 (2019)
- Pages: 531-544
- Section: Article
- URL: https://journals.rcsi.science/1063-7397/article/view/187282
- DOI: https://doi.org/10.1134/S1063739719080079
- ID: 187282
Cite item
Abstract
In this work the crystal structure and texture of isotropic and anisotropic polycrystalline hexagonal ferrites BaFe12O19 obtained by the method of radiation-thermal sintering (RTS) is studied using X-ray diffraction and X-ray phase analysis. Crude blanks of both isotropic and anisotropic hexaferrites are obtained by the standard method of ceramic technology from the same raw material (Fe2O3 and BaCO3 of the analytical grade brand) and on the same equipment with the only difference being that the anisotropic blanks were pressed in the magnetic field H = 10 kOe. For sintering raw billets, a linear electron accelerator ILU-6 (electron energy Ee = 2.5 MeV) is used (Budker Institute of Nuclear Physics, Siberian Branch, Russian Academy of Sciences). The samples are sintered in air for one hour at 1200, 1250, 1300, and 1350°C. It is shown for the first time that high-quality single-phase isotropic and anisotropic hexaferrites BaFe12O19 can be obtained from raw blanks of a ferritized charge using the RTS technology. The properties of the crystal structure and texture of the obtained objects of the research are described. It is established for the first time that the dependence of the pref.orient.o1 predominant orientation of the crystal texture parameter on the degree of the magnetic texture f in polycrystalline hexagonal barium ferrites of type M is described by the expression pref.orient.o1 = –0.005f + 0.6886.
About the authors
I. M. Isaev
National University of Science and Technology MISIS
Email: drvgkostishyn@mail.ru
Russian Federation, Moscow, 119049
A. A. Bryazgin
Budker Institute of Nuclear Physics, Siberian Branch, Russian Academy of Sciences
Email: drvgkostishyn@mail.ru
Russian Federation, Novosibirsk, 630090
M. V. Korobeynikov
Budker Institute of Nuclear Physics, Siberian Branch, Russian Academy of Sciences
Email: drvgkostishyn@mail.ru
Russian Federation, Novosibirsk, 630090
M. A. Mihaylenko
Budker Institute of Nuclear Physics, Siberian Branch, Russian Academy of Sciences
Email: drvgkostishyn@mail.ru
Russian Federation, Novosibirsk, 630090
M. V. Kalinyuk
Stefanyk Precarpathian National University
Email: drvgkostishyn@mail.ru
Ukraine, Ivano-Frankivs’k, 76025
E. A. Belokon’
National University of Science and Technology MISIS; AO NPP Istok im. Shokina
Email: drvgkostishyn@mail.ru
Russian Federation, Moscow, 119049; Fryazino, Moscow oblast, 141190
V. V. Korovushkin
National University of Science and Technology MISIS
Email: drvgkostishyn@mail.ru
Russian Federation, Moscow, 119049
A. A. Alekseev
National University of Science and Technology MISIS; AO NPP Istok im. Shokina
Email: drvgkostishyn@mail.ru
Russian Federation, Moscow, 119049; Fryazino, Moscow oblast, 141190
B. K. Ostafijchuk
Stefanyk Precarpathian National University
Email: drvgkostishyn@mail.ru
Ukraine, Ivano-Frankivs’k, 76025
V. V. Mokljak
Kurdyumov Institute for Metal Physics, National Academy of Sciences
Email: drvgkostishyn@mail.ru
Ukraine, Kiev, 03680
A. G. Nalogin
AO NPP Istok im. Shokina
Email: drvgkostishyn@mail.ru
Russian Federation, Fryazino, Moscow oblast, 141190
V. G. Kostishin
National University of Science and Technology MISIS
Author for correspondence.
Email: drvgkostishyn@mail.ru
Russian Federation, Moscow, 119049
S. V. Shcherbakov
AO NPP Istok im. Shokina
Email: drvgkostishyn@mail.ru
Russian Federation, Fryazino, Moscow oblast, 141190
D. V. Salogub
National University of Science and Technology MISIS
Email: drvgkostishyn@mail.ru
Russian Federation, Moscow, 119049