Determination of glycols in glycol-containing oligomers using gas-liquid reaction chromatography
- 作者: Pervova M.1, Plotnikova K.1, Chizhov D.1, Pestov A.1, Saloutin V.1
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隶属关系:
- Institute of Organic Synthesis, Ural Branch
- 期: 卷 71, 编号 6 (2016)
- 页面: 630-636
- 栏目: Articles
- URL: https://journals.rcsi.science/1061-9348/article/view/181825
- DOI: https://doi.org/10.1134/S1061934816060137
- ID: 181825
如何引用文章
详细
A method is proposed for the gas-chromatographic determination of glycols as bis(diethoxyphosphoryl) alkanes formed by the Atherton–Todd reaction with diethyl phosphite. Gas-chromatographic and mass-spectrometric characteristics of the derivatives obtained are studied. Conditions of the phosphorylation reaction are optimized. The method is applied to the determination of the residual amounts of glycols in oligomeric glycol-o-phthalates.
作者简介
M. Pervova
Institute of Organic Synthesis, Ural Branch
编辑信件的主要联系方式.
Email: pervova@ios.uran.ru
俄罗斯联邦, ul. S. Kovalevskoi 22/Akademicheskaya 20, Yekaterinburg, 620990
K. Plotnikova
Institute of Organic Synthesis, Ural Branch
Email: pervova@ios.uran.ru
俄罗斯联邦, ul. S. Kovalevskoi 22/Akademicheskaya 20, Yekaterinburg, 620990
D. Chizhov
Institute of Organic Synthesis, Ural Branch
Email: pervova@ios.uran.ru
俄罗斯联邦, ul. S. Kovalevskoi 22/Akademicheskaya 20, Yekaterinburg, 620990
A. Pestov
Institute of Organic Synthesis, Ural Branch
Email: pervova@ios.uran.ru
俄罗斯联邦, ul. S. Kovalevskoi 22/Akademicheskaya 20, Yekaterinburg, 620990
V. Saloutin
Institute of Organic Synthesis, Ural Branch
Email: pervova@ios.uran.ru
俄罗斯联邦, ul. S. Kovalevskoi 22/Akademicheskaya 20, Yekaterinburg, 620990
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