Determination of gold and palladium in rocks and ores by atomic absorption spectrometry using two-stage probe atomization
- Autores: Volzhenin A.1, Petrova N.1, Medvedev N.1, Irisov D.2, Saprykin A.1,3
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Afiliações:
- Nikolaev Institute of Inorganic Chemistry, Siberian Branch
- Kazan Federal University
- Novosibirsk State University
- Edição: Volume 72, Nº 2 (2017)
- Páginas: 156-162
- Seção: Articles
- URL: https://journals.rcsi.science/1061-9348/article/view/182296
- DOI: https://doi.org/10.1134/S1061934817020150
- ID: 182296
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Resumo
The efficiency of two-stage probe atomization for the determination of gold and palladium in geological samples by electrothermal atomic absorption spectrometry is studied. The effects of temperature–time program and the position of the probe in an atomizer on the fractionation of sample components and the magnitude of the analytical signal are studied. It is demonstrated that gold and palladium can be quantitatively determined by atomic absorption spectrometry in rocks and ores, using a two-stage probe atomization with the limits of detection for gold and palladium 0.01 and 0.04 g/t, respectively.
Sobre autores
A. Volzhenin
Nikolaev Institute of Inorganic Chemistry, Siberian Branch
Autor responsável pela correspondência
Email: volzhenin@niic.nsc.ru
Rússia, Novosibirsk, 630090
N. Petrova
Nikolaev Institute of Inorganic Chemistry, Siberian Branch
Email: volzhenin@niic.nsc.ru
Rússia, Novosibirsk, 630090
N. Medvedev
Nikolaev Institute of Inorganic Chemistry, Siberian Branch
Email: volzhenin@niic.nsc.ru
Rússia, Novosibirsk, 630090
D. Irisov
Kazan Federal University
Email: volzhenin@niic.nsc.ru
Rússia, Kazan, 420008
A. Saprykin
Nikolaev Institute of Inorganic Chemistry, Siberian Branch; Novosibirsk State University
Email: volzhenin@niic.nsc.ru
Rússia, Novosibirsk, 630090; Novosibirsk, 630090