Determination of iodotyrosines in food


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Resumo

A procedure is developed for the determination of iodinated amino acid residues—iodotyrosines—in food. The procedure is based on the hydrolysis of proteins of a food sample (meat, dairy products, bakery products, canned juices, etc.) followed by purification by solid-phase extraction. Analytes 3-iodo-L-tyrosine and 3,5-diiodo-L-tyrosine were determined by HPLC with mass spectrometric detection. The parameters of the chromatographic separation of iodotyrosines and the conditions of electrospray ionization are presented.

Sobre autores

A. Kulikovskii

Volga Research Institute of Production and Processing of Meat and Dairy Products

Autor responsável pela correspondência
Email: kulikovsky87@gmail.com
Rússia, ul. im. Marshala Rokossovskogo 6, Volgograd, 6400131

A. Lisitsyn

Volga Research Institute of Production and Processing of Meat and Dairy Products

Email: kulikovsky87@gmail.com
Rússia, ul. im. Marshala Rokossovskogo 6, Volgograd, 6400131

I. Chernukha

Gorbatov All-Russia Research Institute of Meat Industry

Email: kulikovsky87@gmail.com
Rússia, Moscow, 109316

I. Gorlov

Volga Research Institute of Production and Processing of Meat and Dairy Products

Email: kulikovsky87@gmail.com
Rússia, ul. im. Marshala Rokossovskogo 6, Volgograd, 6400131

S. Savchuk

I.M. Sechenov First Moscow State Medical University

Email: kulikovsky87@gmail.com
Rússia, Moscow, 119991


Declaração de direitos autorais © Pleiades Publishing, Ltd., 2016

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