Simultaneous Determination of Anthraquinone and Bisphenol A in Pulp and Paper Products by High Performance Liquid Chromatography‒Tandem Mass Spectrometry
- Авторлар: Amosov A.1, Ul’yanovskii N.1, Kosyakov D.1
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Мекемелер:
- Lomonosov Northern (Arctic) Federal University, Core Facility Center “Arktika”
- Шығарылым: Том 74, № 11 (2019)
- Беттер: 1089-1095
- Бөлім: Articles
- URL: https://journals.rcsi.science/1061-9348/article/view/183333
- DOI: https://doi.org/10.1134/S1061934819110029
- ID: 183333
Дәйексөз келтіру
Аннотация
A procedure for the rapid simultaneous determination of anthraquinone and bisphenol A in paper and cardboard is proposed based on a combination of extraction with subcritical methanol and subsequent analysis of the extracts by HPLC‒tandem mass spectrometry. The achieved limits of detection are 25 and 250 µg/kg for anthraquinone and bisphenol A, respectively, and fully meet present-day safety requirements for pulp and paper products. The total duration of the analysis, including sample preparation, is not more than 45 min. The sensitivity of anthraquinone determination is 1‒2 orders of magnitude higher than that of the known procedures, including those with the preconcentration of analytes. The results obtained were successfully used to study paper and cardboard samples, in most of which unacceptably high levels of the anthraquinone concentration were found.
Негізгі сөздер
Авторлар туралы
A. Amosov
Lomonosov Northern (Arctic) Federal University, Core Facility Center “Arktika”
Email: d.kosyakov@narfu.ru
Ресей, Arkhangelsk, 163002
N. Ul’yanovskii
Lomonosov Northern (Arctic) Federal University, Core Facility Center “Arktika”
Email: d.kosyakov@narfu.ru
Ресей, Arkhangelsk, 163002
D. Kosyakov
Lomonosov Northern (Arctic) Federal University, Core Facility Center “Arktika”
Хат алмасуға жауапты Автор.
Email: d.kosyakov@narfu.ru
Ресей, Arkhangelsk, 163002
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