Email this article Identification and determination of mycotoxins and food additives in feed by HPLC–high-resolution time-of-flight mass spectrometry
- Authors: Amelin V.G.1,2, Timofeev A.A.1,2
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Affiliations:
- Federal Centre for Animal Health
- Vladimir State University
- Issue: Vol 71, No 4 (2016)
- Pages: 410-417
- Section: Articles
- URL: https://journals.rcsi.science/1061-9348/article/view/181655
- DOI: https://doi.org/10.1134/S106193481604002X
- ID: 181655
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Abstract
High-resolution time-of-flight mass spectrometry combined with high performance liquid chromatography is proposed for the detection and determination of 25 mycotoxins and 8 food additives (coccidiostats) in animal feed, using simplified and rapid sample preparation. We developed a procedure for the identification and determination of analytes by the standard addition method. The lower limit of the analytical range is 1 (400) µg/kg for mycotoxins; the analytical range for coccidiostats in feed is 10–200 mg/kg. The relative standard deviation of the results does not exceed 10%. The analysis time is 0.5–1 h.
About the authors
V. G. Amelin
Federal Centre for Animal Health; Vladimir State University
Author for correspondence.
Email: amelinvg@mail.ru
Russian Federation, Vladimir, 600901; ul. Gor’kogo 87, Vladimir, 600000
A. A. Timofeev
Federal Centre for Animal Health; Vladimir State University
Email: amelinvg@mail.ru
Russian Federation, Vladimir, 600901; ul. Gor’kogo 87, Vladimir, 600000
