Rare-Earth Nitrate Complexes with Dimethylformamide
- 作者: Petrichko M.1, Karavaev I.1, Savinkina E.1, Grigoriev M.2, Buzanov G.3, Retivov V.4
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隶属关系:
- Lomonosov Institute of Fine Chemical Technologies, MIREA –Russian Technological University
- Frumkin Institute of Physical Chemistry and Electrochemistry, Russian Academy of Sciences
- Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences
- National Research Center “Kurchatov Institute,”
- 期: 卷 68, 编号 4 (2023)
- 页面: 482-491
- 栏目: КООРДИНАЦИОННЫЕ СОЕДИНЕНИЯ
- URL: https://journals.rcsi.science/0044-457X/article/view/136321
- DOI: https://doi.org/10.31857/S0044457X22601821
- EDN: https://elibrary.ru/FLPBBR
- ID: 136321
如何引用文章
详细
In the rare-earth element nitrate (REE)–dimethylformamide (DMF)–water systems, which can be used to obtain nanosized REE oxides by solution combustion synthesis (SCS), the formation of coordination compounds [M(H2O)3(DMF)(NO3)3]·H2O (M = La–Pr) and [M(DMF)3(NO3)3] (M = Sm–Lu, Y) has been found. Using physicochemical methods of analysis (IR spectroscopy, X-ray powder diffraction, single-crystal X-ray diffraction, elemental analysis, thermogravimetric analysis, and differential scanning calorimetry), their composition has been determined and structural features have been established; thermolysis processes have been studied in a wide temperature range. It is shown that the final products of the decomposition of complex compounds are oxides of rare earth elements.
作者简介
M. Petrichko
Lomonosov Institute of Fine Chemical Technologies, MIREA –Russian Technological University
Email: savinkina@mirea.ru
119571, Moscow, Russia
I. Karavaev
Lomonosov Institute of Fine Chemical Technologies, MIREA –Russian Technological University
Email: savinkina@mirea.ru
119571, Moscow, Russia
E. Savinkina
Lomonosov Institute of Fine Chemical Technologies, MIREA –Russian Technological University
Email: savinkina@mirea.ru
119571, Moscow, Russia
M. Grigoriev
Frumkin Institute of Physical Chemistry and Electrochemistry, Russian Academy of Sciences
Email: savinkina@mirea.ru
119071, Moscow, Russia
G. Buzanov
Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences
Email: savinkina@mirea.ru
119991, Moscow, Russia
V. Retivov
National Research Center “Kurchatov Institute,”
编辑信件的主要联系方式.
Email: savinkina@mirea.ru
123182, Moscow, Russia
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