Effect of Substituent Position on Saturated Vapor Pressure of Tetrafluorosubstituted Zinc Phthalocyanines
- Autores: Bonegardt D.1, Trubin S.1, Sukhikh A.1, Klyamer D.1, Basova T.1
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Afiliações:
- Nikolaev Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences
- Edição: Volume 68, Nº 2 (2023)
- Páginas: 181-190
- Seção: КООРДИНАЦИОННЫЕ СОЕДИНЕНИЯ
- URL: https://journals.rcsi.science/0044-457X/article/view/136453
- DOI: https://doi.org/10.31857/S0044457X22601614
- EDN: https://elibrary.ru/LQZYWW
- ID: 136453
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Resumo
This work is devoted to the study of the effect of the position of fluorine substituents in the molecules of tetrafluorosubstituted zinc phthalocyanines on their saturated vapor pressure. For this purpose, the temperature dependence of the saturated vapor pressure of zinc phthalocyanines with fluorine substituents in the peripheral (ZnPcF4-p) and non-peripheral (ZnPcF4-np) positions of the phthalocyanine ring has been studied by the Knudsen method with mass spectrometric recording of the composition of the gas phase and the thermodynamic parameters of vaporization were calculated. The data obtained for ZnPcF4-p and ZnPcF4-np with unsubstituted and hexadecafluorosubstituted zinc phthalocyanines are compared in terms of analysis of intermolecular interactions in the crystals of these compounds. It has been shown that tetrafluorosubstituted phthalocyanines have a higher vapor pressure than their unsubstituted (ZnPc) and hexadecafluorosubstituted (ZnPcF16) derivatives. In this case, the enthalpy of sublimation increases in the series ZnPcF4-p < ZnPcF4-np < ZnPc < ZnPcF16.
Sobre autores
D. Bonegardt
Nikolaev Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences
Email: basova@niic.nsc.ru
630090, Novosibirsk, Russia
S. Trubin
Nikolaev Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences
Email: basova@niic.nsc.ru
630090, Novosibirsk, Russia
A. Sukhikh
Nikolaev Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences
Email: basova@niic.nsc.ru
630090, Novosibirsk, Russia
D. Klyamer
Nikolaev Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences
Email: basova@niic.nsc.ru
630090, Novosibirsk, Russia
T. Basova
Nikolaev Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences
Autor responsável pela correspondência
Email: basova@niic.nsc.ru
630090, Novosibirsk, Russia
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