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Vol 2017, No 10 (2017)

Physical Foundations of Strength and Plasticity

Relaxation of the elastic field of a crystal during the subgrain boundary formation induced by plastic deformation

Sarafanov G.F., Perevezentsev V.N.

Abstract

The change in the energy of a crystal induced by subgrain boundary formation during plastic deformation is studied by computer simulation. The crystal is shown to react to the changes caused by the appearance of plastic misfits: it changes its defect structure to minimize an increase in its elastic energy.

Russian Metallurgy (Metally). 2017;2017(10):775-778
pages 775-778 views

Deformation and Fracture Mechanics

Experimental study and theoretical simulation of the cross hardening effect in shape memory alloys

Movchan A.A., Sil’chenko A.L., Kazarina S.A.

Abstract

The shapes and the relative position of martensitic inelasticity and forward transformation diagrams are experimentally studied. The strain dependences of the stress in loading under martensitic inelasticity conditions after an experiment on the accumulation of the forward transformation–induced strain at a constant or variable stress are investigated on titanium nickelide samples. It is found that the hardening of the martensite part of the representative volume of a shape memory alloy (titanium nickelide) after forward transformation under a nonmonotonically changing stress can be nonuniform. The cross hardening phenomenon is theoretically described in terms of the model of nonlinear deformation of a shape memory alloy during phase and structural transformations.

Russian Metallurgy (Metally). 2017;2017(10):779-784
pages 779-784 views

Advanced Materials and Technologies

Effect of the mechanical activation of a cathode on the structure of electrolytic copper single crystals

Gryzunova N.N., Vikarchuk A.A., Gryzunov A.M., Denisova A.G.

Abstract

The morphology of the electrolytic copper single crystals formed under the mechanical activation of a cathode is described. Pentagonal pyramids and conical microcrystals with high growth steps are shown to form during electrocrystallization under these conditions. It is experimentally found that microcrystals grow on disclination defects, in particular, at the sites of termination of twin growth boundaries, and mechanical activation causes the formation of such defects.

Russian Metallurgy (Metally). 2017;2017(10):785-788
pages 785-788 views

Effect of dynamical chemical etching on the porous structure parameters of superelastic medical Ti–Nb–Zr alloy foam

Sheremetyev V.A., Dubinskiy S.M., Ikbal’ M.A., Korobkova A.A., Kazakbiev A.M., Prokoshkin S.D., Brailovski V.

Abstract

A dynamical chemical etching technique under pressure is developed and used to fabricate sintered foams based on a superelastic Ti–Nb–Zr alloy. This technique is shown to effectively control the characteristics of a porous structure and to increase the porosity and the permeability of the material.

Russian Metallurgy (Metally). 2017;2017(10):789-793
pages 789-793 views

Shape memory effect in a rapidly quenched Ti50Ni25Cu25 alloy

Sitnikov N.N., Shelyakov A.V., Khabibullina I.A., Sundeev R.V.

Abstract

The structural and thermomechanical properties of rapidly quenched layered amorphous–crystalline Ti50Ni25Cu25 composite materials with various ratios of amorphous and crystalline phases are studied. These layered composite materials are shown to exhibit the two-way shape memory effect accompanied by bending deformation without additional thermomechanical treatment. The ratio of amorphous and crystalline phases is found to affect the reversible change in the shape of the composite material.

Russian Metallurgy (Metally). 2017;2017(10):794-800
pages 794-800 views

Structure and magnetic properties of the Nd9.5Fe84.5B6 alloy subjected to severe plastic deformation and annealing

Menushenkov V.P., Shchetinin I.V., Chernykh S.V., Savchenko A.G., Gorshenkov M.V., Zhukov D.G.

Abstract

The effect of severe plastic deformation (SPD) by torsion and subsequent annealing on the structure and magnetic properties of the cast Nd9.5Fe84.5B6 alloy is studied. SPD by torsion is shown to lead to partial amorphization of the Nd2Fe14B phase and the precipitation of α-Fe; subsequent annealing results in the crystallization of the amorphous phase and the formation of a nanocomposite Nd2Fe14B/α-Fe structure. After SPD by torsion at 20 revolutions and annealing at 873 K, the (101) texture is formed; in this case, the coercive force is Hc = 360 kA/m and the maximum energy product is (BH)max = 166 kJ/m3. The residual magnetization and the squareness ratio of the hysteretic loop of the textured alloy decrease as the ambient temperature decreases.

Russian Metallurgy (Metally). 2017;2017(10):801-806
pages 801-806 views

Effect of the milling time on the magnetic properties of powder compositions of the Sm2Fe17Nx intermetallic compound and an Nd–Fe–B alloy

Savchenko A.G., Menushenkov V.P., Plastinin A.Y., Shchetinin I.V., Bordyuzhin I.G., Ryazantsev V.A., Verbetskii V.N., Movlaev E.A.

Abstract

The effect of the wet milling time on the magnetic properties of powder compositions consisting of the hard magnetic Sm2Fe17Nx (x = 2.9–3.0) nitride and a rapidly quenched Nd9.6Fe76.3Co4.3Zr3.4B6.4 (at %) alloy, which are taken in different mass proportions, is studied. The compositions containing no more than 20 wt % alloy are found to exhibit a substantial increase in the magnetic characteristics as compared to those of the nitride. It is shown that the determining effect on the coercivity is related to the degree of structural imperfection of Nd–Fe–B powders, whereas the specific remanent magnetization and the specific magnetization in a field of 2 T are determined by the corresponding characteristics of the alloy. The optimum composition and efficient treatment conditions for powder mixtures are determined.

Russian Metallurgy (Metally). 2017;2017(10):807-812
pages 807-812 views

Structure and Properties of the Deformed State

Methodological aspects of the quantitative texture analysis of HCP Alloy (Ti, Zr) sheet semiproducts

Dzunovich D.A., Betsofen S.Y., Panin P.V.

Abstract

The specific features of the existing methods of quantitative texture analysis of semiproducts and products made of titanium and zirconium alloys are analyzed. A technique is proposed to determine the Kearns coefficients (f parameters) for sheets made of hcp-metal-based alloys with allowance for the weighting factor of each reflection in the standard stereographic triangle. The f parameters calculated for sheets made of a zirconium alloy and various titanium alloys using different techniques are compared. The accuracy of measuring the Kearns coefficients by the inverse pole figure method is estimated.

Russian Metallurgy (Metally). 2017;2017(10):813-820
pages 813-820 views

Role of crushing-induced fragmentation in the consolidation of quartz ceramic and glass powders during high-pressure torsion

Greenberg B.A., Ivanov M.A., Pilyugin V.P., Patselov A.M., Tolmachev T.P.

Abstract

The consolidation of a quartz powders in crystalline (ceramics) and amorphous (glass) states is detected during high-pressure torsion in Bridgman anvils. The consolidation is shown to depend on preceding crushing-induced fragmentation. The role of the surfaces that appear during crushing and cracking is discussed. The dissipative channels that compete with fracture are determined.

Russian Metallurgy (Metally). 2017;2017(10):821-830
pages 821-830 views

Phase composition, texture, and anisotropy of the properties of Al–Cu–Li–Mg alloy sheets

Betsofen S.Y., Antipov V.V., Serebrennikova N.Y., Dolgova M.I., Kabanova Y.A.

Abstract

The formation of the anisotropy of the mechanical properties, the texture, and the phase composition of thin-sheet Al–4.3Cu–1.4Li–0.4Mg and Al–1.8Li–1.8Cu–0.9 Mg alloys have been studied by X-ray diffraction and tensile tests. Various types of anisotropy of the strength properties of the alloys have been revealed: normal anisotropy (strength in the longitudinal direction is higher than that in the transverse direction) in the Al–4.3Cu–1.4Li–0.4Mg alloy and inverse anisotropy in the Al–1.8Li–1.8Cu–0.9Mg alloy. It is shown that the anisotropy of the strength properties is dependent not only on the texture of a solid solution, but also on the content and the texture of the δ' (Al3Li) and T1 (Al2CuLi) phases and their coherency and compatibility of deformation with the matrix.

Russian Metallurgy (Metally). 2017;2017(10):831-837
pages 831-837 views

Anisotropy of the effective elastic modulus of a steel plate with a lattice of circular holes

Gol’dshtein R.V., Mokryakov V.V., Chentsov A.V., Petrovskii V.N., Andreev A.O., Glezer A.M., Libman M.A.

Abstract

Plates with a doubly periodic commensurate lattice of circular holes are studied. The plates are cut from a corrosion-resistant steel sheet along and across the rolling direction. Uniaxial tensile tests are performed, and the effective elastic modulus is determined for longitudinal and transverse plates with various lattice orientations with respect to the longitudinal axis of a plate. The experimental and calculated results agree well.

Russian Metallurgy (Metally). 2017;2017(10):838-841
pages 838-841 views

Shear bands and anisotropy of the mechanical properties of an MA2-1pch magnesium alloy after equal-channel angular pressing

Serebryany V.N., Khar’kova M.A., D’yakonov G.S., Kopylov V.I., Dobatkin S.V.

Abstract

Effect of structure and texture on the anisotropy of the mechanical properties of the MA2-1pch magnesium alloy subjected to equal-channel angular pressing and subsequent annealing has been studied in two mutually perpendicular planes Y and X (along and across the pressing direction). The anisotropy of the mechanical properties is shown to be due to various orientations of shear bands and various types of texture inside the bands and outside them in planes X and Y.

Russian Metallurgy (Metally). 2017;2017(10):842-850
pages 842-850 views

Effect of high-rate deformation on the structure, the properties, and the thermal stability of copper alloyed with chromium and zirconium

Khomskaya I.V., Zel’dovich V.I., Shorokhov E.V., Frolova N.Y., Kheifets A.E., Dyakina V.P.

Abstract

The deformation behavior and the properties of copper alloyed with chromium and zirconium (0.04–0.14 wt %) are studied during high-rate deformation (~105 s–1) by dynamic channel angular pressing (DCAP). The sequence of the decomposition of the α solid solution of copper accompanied by the precipitation of second-phase nanoparticles and recrystallization in annealing (aging) is determined. The influence of DCAP and aging on the mechanical and physical properties of the copper alloys is investigated.

Russian Metallurgy (Metally). 2017;2017(10):851-857
pages 851-857 views

Effect of chromium on the structure evolution in single-phase Ni–Cr alloys during high-pressure torsion

Krasnoperova Y.G., Degtyarev M.V., Chashchukhina T.I., Voronova L.M.

Abstract

The evolution of the structure and the hardness of single-phase Ni–Cr alloys with 2–12.5 at % Cr is studied during high-pressure torsion. It is established that the hardness of the alloys, unlike pure nickel, continuously increases in the entire true strain range 0.2–12. Alloying with chromium is shown to substantially inhibit the formation of a submicrocrystalline structure and to enhance the refinement of microcrystallites.

Russian Metallurgy (Metally). 2017;2017(10):858-861
pages 858-861 views

Applied Problems of Strength and Plasticity

Estimation of the notch sensitivity of a nitrided steel by acoustic emission

Rogachev S.O., Nikulin S.A., Khatkevich V.M., Ozherelkov D.Y., Molyarov A.V.

Abstract

The notch sensitivity of sheet corrosion-resistant 08Kh17T steel is estimated in the states before and after high-temperature (1000–1100°C) internal nitriding during tensile tests accompanied by the measurement of acoustic emission signals. A crack in the steel is shown to propagate according to a ductile mechanism is all states. As the nitrogen content increases from 0.60 to 0.85%, the ultimate tensile strength of the steel decreases by 15% in the presence of a stress concentrator and remains substantially higher than the yield strength of the sheet steel without a stress concentrator.

Russian Metallurgy (Metally). 2017;2017(10):862-866
pages 862-866 views

Influence of the tempering temperature on the mechanical properties and the phase composition of thin sheet TRIP steel

Terent’ev V.F., Eliseev E.A., Matyunin V.M., Slizov A.K., Marchenkov A.Y., Sirotinkin V.P., Baikin A.S., Seval’nev G.S.

Abstract

The strength and the plasticity properties of sheet high-strength austenitic–martensitic VNS9-Sh TRIP steel (23Kh15N5AM3-Sh) are studied as functions of the tempering temperature in the range 125–600°C. A nonmonotonic decease in the strength and the plasticity properties of the steel has been detected when the tempering temperature increases, and they increase in the range 300–450°C. The influence of aging processes, the precipitation of carbide, and the phase transformations in tempering on the mechanical properties of austenitic–martensitic corrosion-resistant steel is discussed.

Russian Metallurgy (Metally). 2017;2017(10):867-870
pages 867-870 views

Evolution of the structure and the phase composition of a bainitic structural steel during plastic deformation

Nikitina E.N., Glezer A.M., Ivanov Y.F., Aksenova K.V., Gromov V.E., Kazimirov S.A.

Abstract

The evolution of the phase composition and the imperfect substructure of the 30Kh2N2MFA bainitic structural steel subjected to compressive deformation by 36% is quantitatively analyzed. It is shown that deformation is accompanied by an increase in the scalar dislocation density, a decrease in the longitudinal fragment sizes, an increase in the number of stress concentrators, the dissolution of cementite particles, and the transformation of retained austenite.

Russian Metallurgy (Metally). 2017;2017(10):871-873
pages 871-873 views

Fracture toughness of as-cast freight bogie solebars after volume–surface quenching

Belov V.A., Nikitin A.V., Anikeenko V.I., Armizonov A.A., Rogachev S.O.

Abstract

The fracture toughness of freight bogie solebars made of low-carbon 20GFL steel is studied in the normalized state and after volume–surface quenching (VSQ). The fracture strength is estimated using acoustic emission and the critical J integral. VSQ is shown to increase Jc of the solebar material by a factor of ≈1.5, and its static strength is higher than that after normalization by ≈1.7 times.

Russian Metallurgy (Metally). 2017;2017(10):874-878
pages 874-878 views

Fracture mechanism of coronal teenage dentin

Panfilov P.E., Kabanova A.V., Borodin I.N., Guo J., Zang Z.

Abstract

The structure of coronal teenage dentin and the development of cracks in it are studied on microand nanolevels. The material is found to fail according to a ductile mechanism on a microlelvel and according to a ductile–brittle mechanism on a nanoscale. This behavior is similar to the failure of a polyethylene film and rubber, when significant elastic and irreversible deformation precedes crack growth. The viscoelastic behavior can be considered as the reaction of dentin to an applied mechanical load.

Russian Metallurgy (Metally). 2017;2017(10):879-883
pages 879-883 views

Adhesion energy in the metal/oxide system for the case of high-temperature oxidation of nickel-based superalloys

Moskvichev V.V., Sukhodoeva N.V., Fedorova E.N., Popov A.S.

Abstract

The microstructure of the oxide layer is studied and the adhesion energy of the metal/oxide interface is determined after high-temperature isothermal oxidation (T = 1150°C) of a single-crystal commercial René N5 nickel alloy. Experiments upon heating and rapid cooling are performed to initiate failure of the oxide layer. The elastic energy of the metal/oxide interface is determined using the model of circular buckling followed by edge delamination. Calculations are conducted for a homogeneous alumina layer and with allowance for the multilayer structure that forms at the initial stages of alloy oxidation. The adhesion energy is 72 and 27 J/m2 for these cases, respectively.

Russian Metallurgy (Metally). 2017;2017(10):884-889
pages 884-889 views

Mechanical and functional properties of commercial alloy TN-1 semiproducts fabricated by warm rotary forging and ECAP

Andreev V.A., Yusupov V.S., Perkas M.M., Prosvirnin V.V., Shelest A.E., Prokoshkin S.D., Khmelevskaya I.Y., Korotitskii A.V., Bondareva S.A., Karelin R.D.

Abstract

The influence of various thermomechanical treatment schemes, which include rotary forging and severe plastic deformation by equal-channel angular pressing, on the structure and the mechanical and functional properties of TiNi alloys is studied. Treatment according to these schemes is shown to result in the formation of a mixed nano- and submicrocrystalline structure with a high dislocation density, which ensures high mechanical (σ0.2 = 760–954 MPa, σu = 917–1097 MPa, δ = 21–51%) and functional (maximum completely recoverable strain of 6.8–8%) properties.

Russian Metallurgy (Metally). 2017;2017(10):890-894
pages 890-894 views

Diagnostics and Mechanical Test Techniques

Analysis of the fracture kinetics and mechanisms of 20GL steel having different strengths using the acoustic emission parameters

Nikulin S.A., Khanzhin V.G., Nikitin A.V., Turilina V.Y., Zabolotnikova V.I.

Abstract

A joint analysis of acoustic emission pulse amplitudes, deformation diagrams, and fracture surfaces is used to study the fracture kinetics and mechanisms of 20GL steel specimens having different hardnesses and cut from the upper fragment of a freight bogie solebar. The fracture of the steel specimens subjected to normalizing and having a uniform strength and ductility over the entire cross section proceeds continuously. The crack that nucleated in the specimens with a gradient strength distribution over the cross section after volume–surface quenching slows down in a layer of a variable strength and ductility and stops in a ductile core. The crack sizes are determined from the measured peak amplitudes of acoustic emission.

Russian Metallurgy (Metally). 2017;2017(10):895-900
pages 895-900 views

Improved method for determining the stress relaxation at the crack tip

Grinevich A.V., Erasov V.S., Avtaev V.V.

Abstract

A technique is suggested to determine the stress relaxation at the crack tip during tests of a specimen of a new type at a constant crack opening fixed by a stay bolt. The shape and geometry of the specimen make it possible to set the load and to determine the crack closure force after long-term exposure using the force transducer of a tensile-testing machine. The stress relaxation at the crack tip is determined in a V95pchT2 alloy specimen at elevated temperatures.

Russian Metallurgy (Metally). 2017;2017(10):901-904
pages 901-904 views

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