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Vol 2016, No 4 (2016)

Physical Foundations of Strength and Plasticity

Generalized grain-size dependence of flow stress

Firstov S.A., Rogul’ T.G., Shut O.A.

Abstract

The grain-size dependence of flow stress upon transition from a micro- to a nanostructured state is analyzed. Characteristic regions with qualitatively different influences of a structure on flow stress are found. Generalized equations have been obtained for the grain-size dependences of yield strength and hardness normalized to Young’s modulus for a wide range of grain sizes using S functions and averaging integrals.

Russian Metallurgy (Metally). 2016;2016(4):257-265
pages 257-265 views

Strange behavior of dislocations of a certain type: Self-locking

Greenberg B.A., Ivanov M.A.

Abstract

The results of studying the self-locking of dislocations, namely, the transformation of glissile dislocations into blocked dislocations in the absence of an applied stress, are generalized. The existence of selflocking is theoretically grounded and experimentally proved via the observation of dislocation extension along a preferred direction upon loading-free heating after preliminary plastic deformation. The following concept is developed to explain the experimental results: an effective force appears in the case of a two-valley dislocation potential relief; it is proportional to the difference between the valley depths and causes the transformation of a dislocation into an indestructible barrier. The temperature anomaly of yield strength and the dislocation self-locking are shown to have the same nature—a two-valley dislocation potential relief. Both effects were observed in Ni3Al- and TiAl-type intermetallics and a pure metal (magnesium).

Russian Metallurgy (Metally). 2016;2016(4):266-285
pages 266-285 views

Promising Materials and Technologies

Thermal stability of the structure of a heat-resistant cobalt alloy hardened with intermetallic γ'-phase precipitates

Epishin A.I., Petrushin N.V., Link T., Nolze G., Loshchinin Y.V., Gerstein G.

Abstract

The thermal stability of the microstructure of a heat-resistant cobalt alloy, which consists of a γ solid solution strengthened with γ'-phase precipitates, has been studied. The temperature behavior of the dissolution of the hardening γ' phase and the kinetics of its coarsening at 700 and 800°C have been determined. It is found that, during prolonged annealing at 800°C, the γ' → β phase transformation occurs.

Russian Metallurgy (Metally). 2016;2016(4):286-291
pages 286-291 views

Superplasticity of beryllium

Papirov I.I., Nikolaenko A.A., Shokurov V.S., Tuzov Y.V.

Abstract

Beryllium is a metal having unique physicomechanical properties, including a record specific rigidity, but it undergoes cold and red brittleness. As a result of long-term investigations, we were the first to manufacture high-purity fine-grained beryllium, which has the room-temperature plasticity that is higher than that of commercial-purity powdered beryllium by an order of magnitude and exhibits superplastic flow at elevated temperatures. In this review, we summarize the results of the long-term study of the superplastic flow of beryllium and the mechanisms of high-temperature deformation.

Russian Metallurgy (Metally). 2016;2016(4):292-299
pages 292-299 views

Calculation-experimental analysis of the thermocyclic deformation of titanium nickelide coil springs

Andronov I.N., Demina M.Y., Polugrudova L.S.

Abstract

The physicomechanical behavior of a cylindrical spring made of titanium nickelide is experimentally studied during thermal cycling through the martensitic transformation ranges at a constant tensile force. The spring exhibits a reversible change in the length and the diameter, the relative change in the length reaches 1476%, and the relative change in the diameter is 33%. The alternation of reciprocating rotary motion and translational motion of the spring is observed during deformation. A method is proposed to estimate the stresses and the strains that appear in the material at large spring elongations. Thermal cycling at a constant axial force is shown to be accompanied by a reversible hysteretic change in the tangential and normal stresses and the shear strains and by a reversible hysteretic reversible change in the axial strains.

Russian Metallurgy (Metally). 2016;2016(4):300-306
pages 300-306 views

Thermomechanical and electrophysical properties of a solid electrolyte based on Na–β"-Al2O3 with t-ZrO2 additions

Sitnikov A.I., Tel’nova G.B., Baikin A.S., Solntsev K.A.

Abstract

The strength, the fracture toughness, the thermal shock resistance, and the electrical conductivity of a ceramic Na–β"-Al2O3 solid electrolyte modified by t-ZrO2 additions are studied. The influence of the reverse t-ZrO2m-ZrO2 transformation on the mechanical and functional properties of the ceramics is discussed. The ZrO2 addition concentration is found to affect the sodium-ion conductivity of the solid electrolyte and its activation energy. The degree of defect accumulation in the ceramics modified by 8.5 wt % t-ZrO2 is shown to decrease during a thermal shock.

Russian Metallurgy (Metally). 2016;2016(4):307-312
pages 307-312 views

Structure and mechanical properties of a multilayer carbide-hardened niobium composite material fabricated by diffusion welding

Korzhov V.P., Ershov A.E., Stroganova T.S., Prokhorov D.V.

Abstract

The structure, the bending strength, and the fracture mechanism of an artificial niobium-based composite material, which is fabricated by high-pressure diffusion welding of multilayer stacks assembled from niobium foils with a two-sided carbon coating, are studied. The microstructure of the composite material is found to consist of alternating relatively plastic layers of the solid solution of carbon in niobium and hardening niobium carbide layers. The room-temperature proportional limit of the developed composite material is threefold that of the composite material fabricated from coating-free niobium foils using the proposed technology. The proportional limit of the developed composite material and the stress corresponding to the maximum load at 1100°C are 500 and 560 MPa, respectively. The developed material is considered as an alternative to Ni–Al superalloys.

Russian Metallurgy (Metally). 2016;2016(4):313-320
pages 313-320 views

Deformation of graphene layers and phase transformations in the hydrogen nanophase intercalated in them

Nechaev Y.S., Filippova V.P., Tomchuk A.A.

Abstract

The intercalation of a high-density molecular hydrogen nanophase into graphene nanostructures has been studied. The deformation of the graphene layers in the material and the phase transformations of intercalated hydrogen, in particular, the thermoelastic equilibrium of the system, is considered. The possibility of intercalating the nanophase of molecular hydrogen into hydrogenated graphite nanofibers is justified theoretically.

Russian Metallurgy (Metally). 2016;2016(4):321-325
pages 321-325 views

Al–Cu–Li and Al–Mg–Li alloys: Phase composition, texture, and anisotropy of mechanical properties (Review)

Betsofen S.Y., Antipov V.V., Knyazev M.I.

Abstract

The results of studying the phase transformations, the texture formation, and the anisotropy of the mechanical properties in Al–Cu–Li and Al–Mg–Li alloys are generalized. A technique and equations are developed to calculate the amounts of the S1 (Al2MgLi), T1 (Al2CuLi), and δ' (Al3Li) phases. The fraction of the δ' phase in Al–Cu–Li alloys is shown to be significantly higher than in Al–Mg–Li alloys. Therefore, the role of the T1 phase in the hardening of Al–Cu–Li alloys is thought to be overestimated, especially in alloys with more than 1.5% Li. A new model is proposed to describe the hardening of Al–Cu–Li alloys upon aging, and the results obtained with this model agree well with the experimental data. A texture, which is analogous to that in aluminum alloys, is shown to form in sheets semiproducts made of Al–Cu–Li and Al–Mg–Li alloys. The more pronounced anisotropy of the properties of lithium-containing aluminum alloys is caused by a significant fraction of the ordered coherent δ' phase, the deformation mechanism in which differs radically from that in the solid solution.

Russian Metallurgy (Metally). 2016;2016(4):326-341
pages 326-341 views

Deformation behavior of submicrocrystalline aluminum alloys during dynamic loading

Brodova I.G., Petrova A.N., Razorenov S.V., Plekhov O.P., Shorokhov E.V.

Abstract

The structure and the mechanical properties of aluminum V95 and AMts alloys with various grain sizes (from micron to submicron) are studied in a wide range of strain rates (from 10–3 to 105 s–1). Submicrocrystalline (200–600 nm) materials are formed by dynamic channel-angular pressing at a strain rate of 105 s–1 using a pulsed power source.

Russian Metallurgy (Metally). 2016;2016(4):342-348
pages 342-348 views

Structure and Properties of the Deformed State

X-ray diffraction measurements of the internal stresses in coarse-grained polycrystals

Lyuttsau A.V., Nikulin S.A.

Abstract

The possibilities of a one-crystal X-ray diffraction analysis of coarse-grained polycrystalline materials are demonstrated for cast 20L steel specimens in order to determine the elastic lattice strains and the residual stresses calculated from them.

Russian Metallurgy (Metally). 2016;2016(4):349-353
pages 349-353 views

Effect of deformation on the structural state of piracetam

Kanunnikova O.M., Mikhailova S.S., Karban’ O.V., Mukhgalin V.V., Aksenova V.V., Sen’kovskii B.V., Pechina E.A., Lad’yanov V.I.

Abstract

The effect of various deformation actions on the structure–phase transformations in piracetam of modifications I and II with a sodium acetate addition is studied. Mechanical activation and pressing are shown to cause the polymorphic transformation of modification I into modification II, and modification III forms predominantly during severe plastic deformation by torsion. The structural difference between the piracetam molecules of modifications I and II is found to be retained in aqueous solutions.

Russian Metallurgy (Metally). 2016;2016(4):354-360
pages 354-360 views

Effect of the phase composition of the surface layer on the mechanical properties of 23Kh15N5AM3-Sh TRIP steel sheets

Terent’ev V.F., Slizov A.K., Prosvirnin D.V., Sirotinkin V.P., Ashmarin A.A., Eliseev E.A., Rybal’chenko O.V.

Abstract

The static and cyclic mechanical properties of cold-rolled corrosion-resistant VNS 9-Sh (23Kh15N5AM3-Sh) TRIP sheet steel from two batches having different deformation martensite contents in the surface layer are studied. An increase in the deformation martensite content is shown to cause an increase in the strength properties, a certain decrease in the plasticity, and an increase in the fatigue limit at 107 cycles.

Russian Metallurgy (Metally). 2016;2016(4):361-364
pages 361-364 views

Laws of the deformation-induced structural transformation in bainitic steel

Ivanov Y.F., Nikitina E.N., Gromov V.E., Glezer A.M., Alsaraeva K.V.

Abstract

The evolution of the defect and carbide subsystems of steel with a bainitic structure during deformation by compression is quantitatively analyzed by transmission electron diffraction microscopy and X-ray diffraction. The strain dependences of the parameters of a dislocation substructure and a carbide phase are determined, and the possible causes of stages in their changes are discussed.

Russian Metallurgy (Metally). 2016;2016(4):365-370
pages 365-370 views

Formation of internal stress fields in rails during long-term operation

Peregudov O.A., Morozov K.V., Gromov V.E., Glezer A.M., Ivanov Y.F.

Abstract

The structure and the internal stress fields in R65 rails withdrawn from operation because of side wear after long-term operation are studied and estimated. A high scalar dislocation density (higher by a factor of 1.5–2), the fragmentation of cementite lamellae, and the precipitation of carbide particles are detected in the layers adjacent to the roll surface. The stresses at the boundaries of the particles with the ferrite matrix can exceed the ultimate strength of the steel.

Russian Metallurgy (Metally). 2016;2016(4):371-374
pages 371-374 views

Structure and properties of a layered steel/vanadium alloy/steel composite prepared by high-pressure torsion

Nikulin S.A., Rogachev S.O., Rozhnov A.B., Khatkevich V.M., Nechaikina T.A., Morozov M.V.

Abstract

The microstructure and hardness of a layered steel 08Kh17T/V–10Ti–5Cr/steel 08Kh17T composite, which was prepared by torsion under a high hydrostatic pressure at temperatures of 20, 200, and 400°C, have been studied. Severe plastic deformation under used conditions is shown to provide good joining of layers, which is accompanied by their substantial hardening (from 2.0 to 3.5 times). During deformation at temperatures of 20 and 200°C, fragmentation of the vanadium alloy layer into thinner layers is observed; at 400°C, mainly a plane interface between the vanadium alloy and the steel layers is formed.

Russian Metallurgy (Metally). 2016;2016(4):375-379
pages 375-379 views

Applied Problems of Strength and Plasticity

Effect of hot rolling on the structure and the mechanical properties of nitrogen-bearing austenitic–martensitic 14Kh15AN4M steel

Bannykh O.A., Betsofen S.Y., Lukin E.I., Blinov V.M., Voznesenskaya N.M., Tonysheva O.A., Blinov E.V.

Abstract

The effect of the rolling temperature and strain on the structure and the properties of corrosionresistant austenitic–martensitic 14Kh15AN4M steel is studied. The steel is shown to exhibit high ductility: upon rolling in the temperature range 700–1100°C at a reduction per pass up to 80%, wedge steel specimens are uniformly deformed along and across the rolling direction without cracking and other surface defects. Subsequent cold treatment and low-temperature tempering ensure a high hardness of the steel (50–56 HRC). Austenite mainly contributes to the hardening upon rolling in the temperature range 700–800°C at a reduction of 50–70%, and martensite makes the main contribution at higher temperatures and lower strains. Texture does not form under the chosen deformation conditions, which indicates dynamic recrystallization with the nucleation and growth of grains having no preferential orientation.

Russian Metallurgy (Metally). 2016;2016(4):380-384
pages 380-384 views

Wear resistance of the oxide layers formed on AK9pch silumin by microarc oxidation in an electrolyte modified by silicon dioxide nanoparticles

Polunin A.V., Ivashin P.V., Rastegaev I.A., Borgardt E.D., Krishtal M.M.

Abstract

The structure, the phase composition, the surface morphology, the microhardness, and the tribological characteristics of the oxide layers of various thicknesses formed on AK9pch alloy during microarc oxidation are studied. A positive influence of a small addition (5 g/L) of nanosized silicon dioxide to an electrolyte on these characteristics of the oxide layers is revealed.

Russian Metallurgy (Metally). 2016;2016(4):385-388
pages 385-388 views

Effect of the rolling temperature on the structure and the mechanical properties of high-nitrogen austenitic steels 05Kh21G9N7AMF and 04Kh22G12N4AMF

Blinov V.M., Voznesenskaya N.M., Bannykh I.O., Tonasheva O.A., Blinov E.V., Zvereva T.N.

Abstract

The structure and the mechanical properties of high-nitrogen austenitic 05Kh21G9N7AMF (0.56% N) and 04Kh22G12N4AMF (0.49% N) steels have been studied after hot rolling. It is found that the temperatures of the onset and end of hot deformation influence the structure and the mechanical properties of these steels. The higher set of mechanical properties of steel 05Kh21G9N7AMF after rolling in the temperature range 1100–900°C is due to the formation of a lamellar and equiaxed fragmented structure.

Russian Metallurgy (Metally). 2016;2016(4):389-393
pages 389-393 views

Fatigue strength of low-activation ferritic–martensitic high-chromium EK-181 steel

Kolmakov A.G., Terent’ev V.F., Prosvirnin D.V., Chernov V.M., Leont’eva-Smirnova M.V.

Abstract

The static and cyclic mechanical properties of low-activation ferritic–martensitic EK-181 (Fe‒12Cr–2W–V–Ta–B–C) steel are studied in the temperature range 20–920°C (static tests) and at 20°C (cyclic tests). The fracture mechanisms of the steel under static tension and fatigue fracture conditions are analyzed by scanning electron microscopy.

Russian Metallurgy (Metally). 2016;2016(4):394-398
pages 394-398 views

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