Liquid-Phase Synthesis and Investigation of Powders Based on Zirconium Dioxide


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Resumo

Xerogels in the ZrO2(Y2O3)–Al2O3 system are obtained by the coprecipitation method followed by a low-temperature treatment at –25°C for 24 h. The physicochemical properties of the powders of ZrO2(Y2O3)–xAl2O3 (х = 15, 20, and 25 mol %) compositions obtained by burning the xerogels are studied. It is shown that the introduction of 25 mol % of Al2O3 promotes the deceleration of the growth of the particles of the t-ZrO2(Y2O3) tetragonal solid solution. It is established that the obtained powders are characterized by high values of the degree of tetragonality (c/a = 1.438–1.436).

Sobre autores

N. Kovalko

Grebenshchikov Institute of Silicate Chemistry, Russian Academy of Sciences

Autor responsável pela correspondência
Email: kovalko.n.yu@gmail.com
Rússia, St. Petersburg, 199034

A. Dolgin

Grebenshchikov Institute of Silicate Chemistry, Russian Academy of Sciences; St. Petersburg State Institute of Technology

Email: kovalko.n.yu@gmail.com
Rússia, St. Petersburg, 199034; St. Petersburg, 190013

L. Efimova

Grebenshchikov Institute of Silicate Chemistry, Russian Academy of Sciences

Email: kovalko.n.yu@gmail.com
Rússia, St. Petersburg, 199034

M. Arsent’ev

Grebenshchikov Institute of Silicate Chemistry, Russian Academy of Sciences

Email: kovalko.n.yu@gmail.com
Rússia, St. Petersburg, 199034

O. Shilova

Grebenshchikov Institute of Silicate Chemistry, Russian Academy of Sciences; St. Petersburg State Institute of Technology; St. Petersburg State Electrotechnical University

Email: kovalko.n.yu@gmail.com
Rússia, St. Petersburg, 199034; St. Petersburg, 190013; St. Petersburg, 197376


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