Formation of 6-aryl-2-methyl-4-oxo- N , N ’-diphenyl-2-cyclohexene-1,3-dicarboxamides from acetoacetanilide and aromatic aldehydes catalyzed by a mixture of aryl amines and iodine

V. L. Gein; A. N. Yankin; N. V. Nosova; M. V. Dmitriev; O. E. Nasakin

doi:10.1134/S1070363216010114

Formation of 6-aryl-2-methyl-4-oxo-N,N’-diphenyl-2-cyclohexene-1,3-dicarboxamides from acetoacetanilide and aromatic aldehydes catalyzed by a mixture of aryl amines and iodine

作者: Gein V.¹, Yankin A.¹, Nosova N.¹, Dmitriev M.², Nasakin O.³
隶属关系:
1. Perm State Pharmaceutical Academy
2. Perm State National Research University
3. Ul’yanov Chuvash State University
期: 卷 86, 编号 1 (2016)
页面: 58-61
栏目: Article
URL: https://journals.rcsi.science/1070-3632/article/view/213416
DOI: https://doi.org/10.1134/S1070363216010114
ID: 213416

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Reactions of acetoacetanilide with aromatic aldehydes in ethanol at room temperature in the presence of molecular iodine and arylamine afford to 6-aryl-2-methyl-4-oxo-N,N’-diphenyl-2-cyclohexene-1,3-dicarboxamides. The structure of obtained compounds was confirmed by mass spectrometry, IR and NMR spectroscopy data.