Self-assembling in the systems МХ 2 –2-(7-bromo-2-oxo-5-phenyl-2,3-dihydro-1 Н -1,4-benzdiazepin-1-yl)acetohydrazide–salicyl aldehyde (М = Сo, Ni, Zn; X = Cl, CH 3 COO)

A. V. Pulya; I. I. Seifullina; L. S. Skorokhod; V. G. Vlasenko; A. L. Trigub; Ya. V. Zubavichus; S. I. Levchenkov

doi:10.1134/S1070363217010145

Self-assembling in the systems МХ₂–2-(7-bromo-2-oxo-5-phenyl-2,3-dihydro-1Н-1,4-benzdiazepin-1-yl)acetohydrazide–salicyl aldehyde (М = Сo, Ni, Zn; X = Cl, CH₃COO)

Authors: Pulya A.V.¹, Seifullina I.I.¹, Skorokhod L.S.¹, Vlasenko V.G.², Trigub A.L.³, Zubavichus Y.V.³, Levchenkov S.I.⁴
Affiliations:
1. I.I. Mechnikov Odessa National University
2. Research Institute of Physics
3. Russian Scientific Center “Kurchatov Institute”
4. Southern Scientific Center
Issue: Vol 87, No 1 (2017)
Pages: 86-91
Section: Article
URL: https://journals.rcsi.science/1070-3632/article/view/217899
DOI: https://doi.org/10.1134/S1070363217010145
ID: 217899

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Abstract

By self-assembling in the systems MX₂–2-(7-bromo-2-oxo-5-phenyl-2,3-dehydro-1Н-1,4-benzdiazepin-1-yl)acetohydrazide (Hydr)–salicyl aldehyde (HSal) (М = Co, Ni, Zn; X = Cl, CH₃COO) the complexes of composition [Co(HydrSal)₂], [Ni(HydrSal)₂], [Zn(HydrHSal)Cl₂], [Zn(HydrSal)(CH₃COO)(H₂O)] have been synthesized. The local atomic structure of the coordination unit was determined by the method of X-ray absorption spectroscopy. Thermal stability, electroconductivity, and magnetic susceptibility of the complexes have been studied.

Keywords

coordination compounds, cobalt(II), nickel(II), zinc(II), 2-(7-bromo-2-oxo-5-phenyl-2,3-dehydro-1Н-1,4-benzdiazepin-1-yl)acetohydrazide, salicylaldehyde

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Self-assembling in the systems МХ2–2-(7-bromo-2-oxo-5-phenyl-2,3-dihydro-1Н-1,4-benzdiazepin-1-yl)acetohydrazide–salicyl aldehyde (М = Сo, Ni, Zn; X = Cl, CH3COO)

Full Text

Abstract

Keywords

About the authors

A. V. Pulya

I. I. Seifullina

L. S. Skorokhod

V. G. Vlasenko

A. L. Trigub

Ya. V. Zubavichus

S. I. Levchenkov

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Self-assembling in the systems МХ₂–2-(7-bromo-2-oxo-5-phenyl-2,3-dihydro-1Н-1,4-benzdiazepin-1-yl)acetohydrazide–salicyl aldehyde (М = Сo, Ni, Zn; X = Cl, CH₃COO)