Solvothermal synthesis of nanosized particles of vanadium oxide


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Abstract

The interaction of vanadyl acetate, vanadium(V) oxide, and vanadium(V) isopropylate with capronic acid has afforded a series of nanosized vanadium oxide powders. The products structure has been studied by X-ray diffraction analysis. Both amorphous and crystalline powders of vanadium oxide can be prepared depending on the starting compound, temperature, and the synthesis duration, the V2O3 (karelianite) structure being in all the cases the most thermodynamically stable. Photocatalytic properties of the prepared powders have been studied.

About the authors

A. V. Zdravkov

Institute of Silicates Chemistry

Email: n.n.khimich@gmail.com
Russian Federation, St. Petersburg

M. A. Gorbunova

St. Petersburg State Technological University of Plant Polymers

Email: n.n.khimich@gmail.com
Russian Federation, St. Petersburg

L. A. Koptelova

Institute of Silicates Chemistry

Email: n.n.khimich@gmail.com
Russian Federation, St. Petersburg

N. N. Khimich

St. Petersburg State Technological University of Plant Polymers; Kirov Military Medical Academy

Author for correspondence.
Email: n.n.khimich@gmail.com
Russian Federation, St. Petersburg; ul. Akademika Lebedeva 6/Zh, St. Petersburg, 194044


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