Enviar artigo por via de e-mail Synthesis of 3-phenylbenzo[c]isoxazoles by thermocyclization of 2-azidobenzophenones
- Autores: Odinokov A.V.1, Plekhovich S.D.1, Budruev A.V.1
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Afiliações:
- Department of Chemistry, N. I. Lobachevsky State University of Nizhny Novgorod
- Edição: Volume 68, Nº 6 (2019)
- Páginas: 1298-1300
- Seção: Brief Communication
- URL: https://journals.rcsi.science/1066-5285/article/view/243418
- DOI: https://doi.org/10.1007/s11172-019-2557-5
- ID: 243418
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Resumo
3-Phenylbenzo[c]isoxazoles were synthesized by non-catalytic thermolysis of 2-azidobenzophenones in dry xylene with quantitative yields. The trace content of water in solvents reduces the yields of the reaction products. 2-Azidobenzoic acid esters are stable under the indicated conditions.
Sobre autores
A. Odinokov
Department of Chemistry, N. I. Lobachevsky State University of Nizhny Novgorod
Email: budruev@gmail.com
Rússia, build. 5, 23, prosp. Gagarina, Nizhny Novgorod, 603950
S. Plekhovich
Department of Chemistry, N. I. Lobachevsky State University of Nizhny Novgorod
Email: budruev@gmail.com
Rússia, build. 5, 23, prosp. Gagarina, Nizhny Novgorod, 603950
A. Budruev
Department of Chemistry, N. I. Lobachevsky State University of Nizhny Novgorod
Autor responsável pela correspondência
Email: budruev@gmail.com
Rússia, build. 5, 23, prosp. Gagarina, Nizhny Novgorod, 603950
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