Synthesis and some transformations of 2-[(4-aminofurazan-3-yl)-1 H -1,2,4-triazol-5-yl]acetic acid derivatives

N. S. Aleksandrova; S. S. Semyakin; A. A. Anisimov; M. I. Struchkova; A. B. Sheremetev

doi:10.1007/s11172-018-2325-y

Synthesis and some transformations of 2-[(4-aminofurazan-3-yl)-1H-1,2,4-triazol-5-yl]acetic acid derivatives

作者: Aleksandrova N.S.¹, Semyakin S.S.¹, Anisimov A.A.², Struchkova M.I.¹, Sheremetev A.B.¹
隶属关系:
1. N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences
2. A. N. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences
期: 卷 67, 编号 11 (2018)
页面: 2035-2043
栏目: Full Articles
URL: https://journals.rcsi.science/1066-5285/article/view/243167
DOI: https://doi.org/10.1007/s11172-018-2325-y
ID: 243167

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Two methods for the synthesis of 1,2,4-triazolylacetic ester bearing an aminofurazanyl substituent at the position 5 were developed. The triazole cycle was formed via the cyclocondensation of 3-aminofurazanecarboxylic acid hydrazide or amidrazone with ethoxycarbonylethyl acetimidate hydrochloride.