Email this article Three-step synthesis of Pd0/TiO2
- Authors: Shishmakov A.B.1, Mikushina Y.V.1, Petrov L.A.1
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Affiliations:
- I. Ya. Postovsky Institute of Organic Synthesis, Ural Branch of the Russian Academy of Sciences
- Issue: Vol 68, No 7 (2019)
- Pages: 1451-1453
- Section: Brief Communications
- URL: https://journals.rcsi.science/1066-5285/article/view/243437
- DOI: https://doi.org/10.1007/s11172-019-2576-2
- ID: 243437
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Abstract
A simplifi ed procedure for the synthesis of Pd0/TiO2 xerogel has been developed, which includes the following steps: hydrolysis of tetrabutoxytitanium from its mixture with a palladium salt in an acetic acid atmosphere, drying and calcining the material at 860 °C. Palladium in the calcined xerogel is present in the form of spherical particles, titanium dioxide — as rutile aggregates.
About the authors
A. B. Shishmakov
I. Ya. Postovsky Institute of Organic Synthesis, Ural Branch of the Russian Academy of Sciences
Email: mikushina@ios.uran.ru
Russian Federation, 22/20 ul. S. Kovalevskoi, Ekaterinburg, 620990
Yu. V. Mikushina
I. Ya. Postovsky Institute of Organic Synthesis, Ural Branch of the Russian Academy of Sciences
Author for correspondence.
Email: mikushina@ios.uran.ru
Russian Federation, 22/20 ul. S. Kovalevskoi, Ekaterinburg, 620990
L. A. Petrov
I. Ya. Postovsky Institute of Organic Synthesis, Ural Branch of the Russian Academy of Sciences
Email: mikushina@ios.uran.ru
Russian Federation, 22/20 ul. S. Kovalevskoi, Ekaterinburg, 620990
