Отправить статью по E-mail Synthesis of nanocomposite with a core—shell structure based on Fe3O4 magnetic nanoparticles and iron glycerolate
- Авторы: Dentin A.M.1, Khonina T.G.1, Shadrina E.V.1, Bogdanova E.A.2, Kuznetsov D.K.3, Mekhaev A.V.1, Shur V.Y.3, Krasnov V.P.1
-
Учреждения:
- Postovsky Institute of Organic Synthesis of the Russian Academy of Sciences (Ural Branch)
- Institute of Solid State Chemistry of the Russian Academy of Sciences (Ural Branch)
- Institute of Natural Sciences and Mathematics, Ural Federal University
- Выпуск: Том 68, № 6 (2019)
- Страницы: 1178-1182
- Раздел: Full Article
- URL: https://journals.rcsi.science/1066-5285/article/view/243397
- DOI: https://doi.org/10.1007/s11172-019-2536-x
- ID: 243397
Цитировать
Открытый доступ
Доступ предоставлен
Только для подписчиков
Аннотация
An original method for preparation of nanoparticles with a core—shell structure based on Fe3O4 magnetic nanoparticles (MNPs) and iron glycerolate was proposed. The formation of a coating on the MNP surface with a diameter of 11 nm was carried out by heating them in glycerol at 220 °C for 40 h. The synthesized nanoparticles were characterized using scanning transmission electron microscopy, XRD and IR spectroscopy. The amount of glycerol fragments in the nanocomposite calculated from the elemental analysis and TGA was 3.6 mmol per 1 g of MNPs (32.08 wt.%).
Об авторах
A. Dentin
Postovsky Institute of Organic Synthesis of the Russian Academy of Sciences (Ural Branch)
Автор, ответственный за переписку.
Email: demin@ios.uran.ru
Россия, 22 ul. S. Kovalevskoi, Ekaterinburg, 620990
T. Khonina
Postovsky Institute of Organic Synthesis of the Russian Academy of Sciences (Ural Branch)
Email: demin@ios.uran.ru
Россия, 22 ul. S. Kovalevskoi, Ekaterinburg, 620990
E. Shadrina
Postovsky Institute of Organic Synthesis of the Russian Academy of Sciences (Ural Branch)
Email: demin@ios.uran.ru
Россия, 22 ul. S. Kovalevskoi, Ekaterinburg, 620990
E. Bogdanova
Institute of Solid State Chemistry of the Russian Academy of Sciences (Ural Branch)
Email: demin@ios.uran.ru
Россия, 91 ul. Pervomaiskaya, Ekaterinburg, 620990
D. Kuznetsov
Institute of Natural Sciences and Mathematics, Ural Federal University
Email: demin@ios.uran.ru
Россия, 51 prosp. Lenina, Ekaterinburg, 620000
A. Mekhaev
Postovsky Institute of Organic Synthesis of the Russian Academy of Sciences (Ural Branch)
Email: demin@ios.uran.ru
Россия, 22 ul. S. Kovalevskoi, Ekaterinburg, 620990
V. Shur
Institute of Natural Sciences and Mathematics, Ural Federal University
Email: demin@ios.uran.ru
Россия, 51 prosp. Lenina, Ekaterinburg, 620000
V. Krasnov
Postovsky Institute of Organic Synthesis of the Russian Academy of Sciences (Ural Branch)
Email: demin@ios.uran.ru
Россия, 22 ul. S. Kovalevskoi, Ekaterinburg, 620990
Дополнительные файлы
