Email this article Preparation and thermal behavior of the formulation of Ftorsam-39 with SKF-26(ONM) fluorine rubber
- Authors: Sakharov A.M.1, Popovich M.Y.1, Krukovsky S.P.1
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Affiliations:
- N. D. Zelinsky Institute of Organic Chemistry Russian Academy of Science
- Issue: Vol 68, No 2 (2019)
- Pages: 449-452
- Section: Brief Communications
- URL: https://journals.rcsi.science/1066-5285/article/view/243268
- DOI: https://doi.org/10.1007/s11172-019-2407-5
- ID: 243268
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Abstract
A synthetic procedure was designed to prepare formulations from Ftorsam-39 monomer (perfluoro-2,5-dimethyl-3,6-dioxanonoic acid triethoxysilylpropylamide) with SKF-26(ONM) fluorine rubber (poly(vinylidene fluoride-co-hexafluoropropylene)) in a presence of AGM-9 (γ-aminopropyltriethoxysilane) as a catalyst and co-reagent. The content of fluorine rubber in the compositions was varied from 10 to 54 wt.%. Thermal properties of the formulations obtained with the ratio Ftorsam-39: SKF-26(ONM): AGM-9 = 40: 54: 6 (wt.%) were assessed using thermomechanical and thermogravimetric analysis and differential scanning calorimetry.
About the authors
A. M. Sakharov
N. D. Zelinsky Institute of Organic Chemistry Russian Academy of Science
Email: yar@ioc.ac.ru
Russian Federation, 47 Leninsky prosp., Moscow, 119991
M. Yu. Popovich
N. D. Zelinsky Institute of Organic Chemistry Russian Academy of Science
Email: yar@ioc.ac.ru
Russian Federation, 47 Leninsky prosp., Moscow, 119991
S. P. Krukovsky
N. D. Zelinsky Institute of Organic Chemistry Russian Academy of Science
Author for correspondence.
Email: yar@ioc.ac.ru
Russian Federation, 47 Leninsky prosp., Moscow, 119991
