Synthesis of 3,3-bis(2-haloethyl) and 3,3,3′-tris(2-haloethyl) derivatives of 1,1′-[methylenebis(oxy)]bis(triaz-1-ene 2-oxides)

T. V. Ternikova; G. V. Pokhvisneva; G. A. Smirnov; P. B. Gordeev; S. V. Nikitin; O. A. Luk’yanov

doi:10.1007/s11172-017-1987-1

Synthesis of 3,3-bis(2-haloethyl) and 3,3,3′-tris(2-haloethyl) derivatives of 1,1′-[methylenebis(oxy)]bis(triaz-1-ene 2-oxides)

Authors: Ternikova T.V.¹, Pokhvisneva G.V.¹, Smirnov G.A.¹, Gordeev P.B.¹, Nikitin S.V.¹, Luk’yanov O.A.¹
Affiliations:
1. N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences
Issue: Vol 66, No 11 (2017)
Pages: 2103-2109
Section: Full Article
URL: https://journals.rcsi.science/1066-5285/article/view/241572
DOI: https://doi.org/10.1007/s11172-017-1987-1
ID: 241572

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Abstract

Synthetic procedures towards 3,3-bis(2-haloethyl) and 3,3,3′-tris(2-haloethyl) derivatives of 1,1′-[methylenebis(oxy)]bis(triaz-1-ene 2-oxides) via halogenation of the corresponding 2-hydroxyethyl derivatives of 1,1′-[methylenebis(oxy)]bis(triaz-1-ene 2-oxides) and iodination of the corresponding 2-bromoethyl derivatives were elaborated. The synthesized compounds are promising NO donors in the living organisms.