Nuclear Magnetic Resonance Spectra of Polyhydroxylated Fullerene C 60 (OH)  n

A. S. Mazur; A. E. Karpunin; O. V. Proskurina; V. I. Gerasimov; I. V. Pleshakov; V. V. Matveev; Yu. I. Kuz’min

doi:10.1134/S106378341807017X

Nuclear Magnetic Resonance Spectra of Polyhydroxylated Fullerene C₆₀(OH)_n

Authors: Mazur A.S.¹, Karpunin A.E.², Proskurina O.V.³^,4, Gerasimov V.I.², Pleshakov I.V.²^,4, Matveev V.V.¹, Kuz’min Y.I.²^,4
Affiliations:
1. St. Petersburg State University
2. St. Petersburg Polytechnic University
3. St. Petersburg State Technological Institute (Technical University)
4. Ioffe Institute
Issue: Vol 60, No 7 (2018)
Pages: 1468-1470
Section: Fullerenes
URL: https://journals.rcsi.science/1063-7834/article/view/203532
DOI: https://doi.org/10.1134/S106378341807017X
ID: 203532

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Abstract

Polyhydroxylated fullerene C₆₀(OH)_n (with an estimated number of hydroxyl groups n = 38–44) synthesized from pure fullerene by mixing a benzene solution of C₆₀ with a NaOH aqueous solution in the presence of a catalyst was studied with ¹H and ¹³C solid-state nuclear magnetic resonance. Possible features of the structure of a molecule shell were revealed from ¹H NMR data. The ¹³C spectrum showed a peak splitting with an increase in temperature, which is probably due to fullerenol isomers.

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Nuclear Magnetic Resonance Spectra of Polyhydroxylated Fullerene C60(OH)n

Full Text

Abstract

About the authors

A. S. Mazur

A. E. Karpunin

O. V. Proskurina

V. I. Gerasimov

I. V. Pleshakov

V. V. Matveev

Yu. I. Kuz’min

Supplementary files

Nuclear Magnetic Resonance Spectra of Polyhydroxylated Fullerene C₆₀(OH)_n